{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1050300533201740416.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"HDL","@value":"https://hdl.handle.net/20.500.14094/0100489960"}},{"identifier":{"@type":"DOI","@value":"10.1016/j.jorganchem.2024.123162"}},{"identifier":{"@type":"URI","@value":"https://api.elsevier.com/content/article/PII:S0022328X24001578?httpAccept=text/xml"}},{"identifier":{"@type":"URI","@value":"https://api.elsevier.com/content/article/PII:S0022328X24001578?httpAccept=text/plain"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@language":"en","@value":"Preparation, thermal properties, and structures of ionic plastic crystals with sandwich and half-sandwich Ru complexes"}],"dc:language":"en","description":[{"type":"Abstract","notation":[{"@language":"en","@value":"We have recently been investigating the phase behavior of salts of cationic sandwich complexes in pursuit of novel ionic plastic crystals (IPCs). In this study, we synthesized salts containing sandwich complexes [Ru(Cp)(C₆H₆)]X ([1]X; X = CPFSA⁻ (1,1,2,2,3,3-hexafluoropropane-1,3-disulfonimide), SbCl₆⁻) and half-sandwich complexes [Ru(Cp)(DMSO)₃]X ([2]X; X = CPFSA⁻, FSA⁻ ((FSO₂)₂N⁻), PF₆⁻). In addition, we examined their thermal properties and crystal structures. Among them, [1]CPFSA exhibited an IPC phase between 365 and 630 K, whereas the others did not undergo phase transitions at 123–403 K. The cations and anions were alternately arranged in the crystals of [1]X, whereas [2]X did not exhibit the alternating arrangement except for [2]PF₆. The results showed that alternating molecular arrangements are crucial for the IPC formation, although low symmetry of the ion environment and intermolecular steric hindrance may inhibit it."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1070300533201740416","@type":"Researcher","foaf:name":[{"@language":"en","@value":"Inoue, Ryota"}]},{"@id":"https://cir.nii.ac.jp/crid/1070300533201740418","@type":"Researcher","foaf:name":[{"@language":"en","@value":"Sumitani, Ryo"}]},{"@id":"https://cir.nii.ac.jp/crid/1420001326219183488","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"30280580"},{"@type":"NRID","@value":"1000030280580"},{"@type":"ORCID","@value":"0000-0002-3446-2145"},{"@type":"NRID","@value":"9000003264949"},{"@type":"NRID","@value":"9000279203359"},{"@type":"NRID","@value":"9000401902166"},{"@type":"NRID","@value":"9000401887474"},{"@type":"NRID","@value":"9000258195140"},{"@type":"NRID","@value":"9000414199295"},{"@type":"NRID","@value":"9000251870636"},{"@type":"NRID","@value":"9000239605081"},{"@type":"NRID","@value":"9000239605115"},{"@type":"NRID","@value":"9000387917010"},{"@type":"NRID","@value":"9000282391352"},{"@type":"NRID","@value":"9000413929441"},{"@type":"NRID","@value":"9000401896206"},{"@type":"NRID","@value":"9000402215319"},{"@type":"NRID","@value":"9000308368346"},{"@type":"NRID","@value":"9000239605126"},{"@type":"NRID","@value":"9000239605065"},{"@type":"NRID","@value":"9000332701966"},{"@type":"NRID","@value":"9000397707185"},{"@type":"NRID","@value":"9000403323781"},{"@type":"NRID","@value":"9000258195593"},{"@type":"NRID","@value":"9000292872378"},{"@type":"NRID","@value":"9000239605112"},{"@type":"NRID","@value":"9000239605110"},{"@type":"NRID","@value":"9000239605028"},{"@type":"NRID","@value":"9000332701961"},{"@type":"NRID","@value":"9000390880570"},{"@type":"NRID","@value":"9000401901150"},{"@type":"NRID","@value":"9000258187349"},{"@type":"NRID","@value":"9000001898468"},{"@type":"NRID","@value":"9000267768925"},{"@type":"NRID","@value":"9000239605085"},{"@type":"NRID","@value":"9000239605084"},{"@type":"NRID","@value":"9000239605255"},{"@type":"NRID","@value":"9000332701765"},{"@type":"NRID","@value":"9000365496914"},{"@type":"NRID","@value":"9000383699718"},{"@type":"NRID","@value":"9000347163417"},{"@type":"NRID","@value":"9000413945309"},{"@type":"NRID","@value":"9000251870626"},{"@type":"NRID","@value":"9000239605070"},{"@type":"NRID","@value":"9000332701964"},{"@type":"NRID","@value":"9000401885918"},{"@type":"NRID","@value":"9000401886815"},{"@type":"NRID","@value":"9000257732475"},{"@type":"NRID","@value":"9000278465549"},{"@type":"NRID","@value":"9000107352187"},{"@type":"NRID","@value":"9000252748453"},{"@type":"NRID","@value":"9000239605105"},{"@type":"NRID","@value":"9000239605102"},{"@type":"NRID","@value":"9000410976508"},{"@type":"NRID","@value":"9000404481264"},{"@type":"NRID","@value":"9000399545141"},{"@type":"NRID","@value":"9000398646909"},{"@type":"NRID","@value":"9000239605118"},{"@type":"NRID","@value":"9000392843844"},{"@type":"NRID","@value":"9000383699727"},{"@type":"NRID","@value":"9000346926212"},{"@type":"NRID","@value":"9000345326003"},{"@type":"NRID","@value":"9000258200433"},{"@type":"NRID","@value":"9000292872373"},{"@type":"NRID","@value":"9000239605075"},{"@type":"NRID","@value":"9000243845464"},{"@type":"NRID","@value":"9000243845461"},{"@type":"NRID","@value":"9000411276060"},{"@type":"NRID","@value":"9000292881730"},{"@type":"NRID","@value":"9000401966436"},{"@type":"NRID","@value":"9000001377285"},{"@type":"NRID","@value":"9000237858069"},{"@type":"NRID","@value":"9000239605109"},{"@type":"NRID","@value":"9000414482112"},{"@type":"NRID","@value":"9000399535461"},{"@type":"NRID","@value":"9000394470937"},{"@type":"NRID","@value":"9000391962770"},{"@type":"NRID","@value":"9000401895080"},{"@type":"NRID","@value":"9000006614820"},{"@type":"NRID","@value":"9000239605122"},{"@type":"NRID","@value":"9000239605089"},{"@type":"NRID","@value":"9000365496907"},{"@type":"NRID","@value":"9000399804314"},{"@type":"NRID","@value":"9000410312511"},{"@type":"NRID","@value":"9000406226754"},{"@type":"NRID","@value":"9000401872040"},{"@type":"NRID","@value":"9000403427738"},{"@type":"NRID","@value":"9000412200570"},{"@type":"NRID","@value":"9000410976440"},{"@type":"NRID","@value":"9000408476154"},{"@type":"NRID","@value":"9000411031453"},{"@type":"NRID","@value":"9000258201348"},{"@type":"NRID","@value":"9000239605103"},{"@type":"NRID","@value":"9000239605113"},{"@type":"NRID","@value":"9000365496900"},{"@type":"NRID","@value":"9000401871231"},{"@type":"NRID","@value":"9000045659881"},{"@type":"NRID","@value":"9000045656142"},{"@type":"NRID","@value":"9000283260209"},{"@type":"NRID","@value":"9000414482109"},{"@type":"NRID","@value":"9000323290775"},{"@type":"NRID","@value":"9000292872376"},{"@type":"NRID","@value":"9000239605095"},{"@type":"NRID","@value":"9000239605094"},{"@type":"NRID","@value":"9000392843851"},{"@type":"NRID","@value":"9000411276057"},{"@type":"NRID","@value":"9000365496909"},{"@type":"NRID","@value":"9000409620348"},{"@type":"NRID","@value":"9000256022406"},{"@type":"NRID","@value":"9000257727183"},{"@type":"KAKEN_RESEARCHERS","@value":"20813439"},{"@type":"NRID","@value":"1000020813439"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/m-ueda"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/tmochida"}],"foaf:name":[{"@language":"en","@value":"Mochida, Tomoyuki"},{"@language":"ja","@value":"持田, 智行"},{"@language":"ja-Kana","@value":"モチダ, トモユキ"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"0022328X"},{"@type":"EISSN","@value":"18728561"}],"prism:publicationName":[{"@language":"en","@value":"Journal of Organometallic Chemistry"}],"dc:publisher":[{"@value":"Elsevier B.V."}],"prism:publicationDate":"2024-06-01","prism:volume":"1013","prism:startingPage":"123162"},"reviewed":"false","dcterms:accessRights":"http://purl.org/coar/access_right/c_abf2","dc:rights":["© 2024 The Author(s). Published by Elsevier B.V.","This is an open access article under the Creative Commons Attribution 4.0 International license"],"url":[{"@id":"https://api.elsevier.com/content/article/PII:S0022328X24001578?httpAccept=text/xml"},{"@id":"https://api.elsevier.com/content/article/PII:S0022328X24001578?httpAccept=text/plain"}],"availableAt":"2024-06-11","foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=Sandwich%20complexes","dc:title":"Sandwich complexes"},{"@id":"https://cir.nii.ac.jp/all?q=Half-sandwich%20complexes","dc:title":"Half-sandwich complexes"},{"@id":"https://cir.nii.ac.jp/all?q=Phase%20transitions","dc:title":"Phase transitions"},{"@id":"https://cir.nii.ac.jp/all?q=Ionic%20plastic%20crystals","dc:title":"Ionic plastic crystals"},{"@id":"https://cir.nii.ac.jp/all?q=Thermal%20properties","dc:title":"Thermal properties"},{"@id":"https://cir.nii.ac.jp/all?q=Crystal%20structures","dc:title":"Crystal structures"}],"dcterms:subject":[{"subjectScheme":"Other","notation":[{"@language":"en","@value":"Sandwich complexes"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"Half-sandwich complexes"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"Phase transitions"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"Ionic plastic crystals"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"Thermal properties"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"Crystal structures"}]}],"project":[{"@id":"https://cir.nii.ac.jp/crid/1040292706166763264","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"22K19049"},{"@type":"JGN","@value":"JP22K19049"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-22K19049/"}],"notation":[{"@language":"ja","@value":"有機金属錯体でプラスチック結晶を創る：柔らかい錯体結晶相の開拓"},{"@language":"en","@value":"Designing Ionic Plastic Crystals from Organometallic Complexes: Toward Soft Crystalline Metal Complexes"}]}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050012570392904704","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Phase transitions and crystal structures of organometallic ionic plastic crystals comprised of ferrocenium cations and CH2BrBF3 anions"}]},{"@id":"https://cir.nii.ac.jp/crid/1050023627022156928","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Organometallic Ionic Plastic Crystals Incorporating Cationic Half-Sandwich Complexes"}]},{"@id":"https://cir.nii.ac.jp/crid/1050024268798128896","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Assembled Structures and Electrical Conductivities of Salts Comprised of Cationic Sandwich Complexes 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[Ru(η5-C5H5)(η6-trans-PhCHCHPh)][PF6]·0.5trans-PhCHCHPh and the reversible order–disorder phase transition in [Ru(η5-C5H5)(η6-C6H6)][PF6]"}]},{"@id":"https://cir.nii.ac.jp/crid/1360574096093900160","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Photoinduced Ligand Isomerization in Dimethyl Sulfoxide Complexes of Ruthenium(II)"}]},{"@id":"https://cir.nii.ac.jp/crid/1360857597240575616","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Harnessing molecular rotations in plastic crystals: a holistic view for crystal engineering of adaptive soft materials"}]},{"@id":"https://cir.nii.ac.jp/crid/1360861712121206016","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Multifunctional properties and multi-energy storage in the [(CH\n                    <sub>3</sub>\n                    )\n                    <sub>3</sub>\n                    S][FeCl\n                    <sub>4</sub>\n              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