{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1050861925321854976.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"HDL","@value":"http://hdl.handle.net/2433/286770"}},{"identifier":{"@type":"DOI","@value":"10.1002/advs.202301876"}},{"identifier":{"@type":"URI","@value":"https://advanced.onlinelibrary.wiley.com/doi/pdf/10.1002/advs.202301876"}},{"identifier":{"@type":"PMID","@value":"37096836"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@language":"en","@value":"Emergence of Dynamically-Disordered Phases During Fast Oxygen Deintercalation Reaction of Layered Perovskite"},{"@value":"Emergence of Dynamically‐Disordered Phases During Fast Oxygen Deintercalation Reaction of Layered Perovskite"}],"dc:language":"en","description":[{"type":"Abstract","notation":[{"@language":"en","@value":"Determination of a reaction pathway is an important issue for the optimization of reactions. However, reactions in solid-state compounds have remained poorly understood because of their complexity and technical limitations. Here, using state-of-the-art high-speed time-resolved synchrotron X-ray techniques, the topochemical solid-gas reduction mechanisms in layered perovskite Sr3Fe2O7−δ (from δ ∼ 0.4 to δ = 1.0), which is promising for an environmental catalyst material is revealed. Pristine Sr3Fe2O7−δ shows a gradual single-phase structural evolution during reduction, indicating that the reaction continuously proceeds through thermodynamically stable phases. In contrast, a nonequilibrium dynamically-disordered phase emerges a few seconds before a first-order transition during the reduction of a Pd-loaded sample. This drastic change in the reaction pathway can be explained by a change in the rate-determining step. The synchrotron X-ray technique can be applied to various solid-gas reactions and provides an opportunity for gaining a better understanding and optimizing reactions in solid-state compounds."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1420564276171014912","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"10749972"},{"@type":"NRID","@value":"1000010749972"},{"@type":"NRID","@value":"9000018756415"},{"@type":"NRID","@value":"9000410023493"},{"@type":"NRID","@value":"9000401968228"},{"@type":"NRID","@value":"9000401507620"},{"@type":"NRID","@value":"9000404336765"},{"@type":"NRID","@value":"9000409646644"},{"@type":"NRID","@value":"9000402819015"},{"@type":"NRID","@value":"9000410310519"},{"@type":"NRID","@value":"9000405705143"},{"@type":"NRID","@value":"9000401965550"},{"@type":"NRID","@value":"9000410310508"},{"@type":"NRID","@value":"9000409646641"},{"@type":"NRID","@value":"9000413697053"},{"@type":"NRID","@value":"9000412115423"},{"@type":"NRID","@value":"9000401976869"},{"@type":"NRID","@value":"9000241541327"},{"@type":"NRID","@value":"9000409885224"},{"@type":"NRID","@value":"9000412381601"},{"@type":"NRID","@value":"9000386095531"},{"@type":"NRID","@value":"9000402032518"},{"@type":"NRID","@value":"9000252667774"},{"@type":"NRID","@value":"9000387366507"},{"@type":"NRID","@value":"9000412322360"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/kshogo"}],"foaf:name":[{"@language":"en","@value":"Kawaguchi, 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Tsunehiro"},{"@language":"ja","@value":"田中, 庸裕"}]},{"@id":"https://cir.nii.ac.jp/crid/1070861925321854976","@type":"Researcher","foaf:name":[{"@language":"en","@value":"Hosokawa, Saburo"},{"@language":"ja","@value":"細川, 三郎"}]},{"@id":"https://cir.nii.ac.jp/crid/1070861925321854980","@type":"Researcher","foaf:name":[{"@language":"en","@value":"Uruga, Tomoya"}]}],"publication":{"publicationIdentifier":[{"@type":"EISSN","@value":"21983844"},{"@type":"PISSN","@value":"21983844"}],"prism:publicationName":[{"@language":"en","@value":"Advanced Science"}],"dc:publisher":[{"@value":"Wiley"}],"prism:publicationDate":"2023-07-06","prism:volume":"10","prism:number":"19","prism:startingPage":"2301876"},"reviewed":"false","dcterms:accessRights":"http://purl.org/coar/access_right/c_abf2","url":[{"@id":"https://advanced.onlinelibrary.wiley.com/doi/pdf/10.1002/advs.202301876"}],"foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=oxygen%20storage%20material","dc:title":"oxygen storage material"},{"@id":"https://cir.nii.ac.jp/all?q=perovskite%20oxide","dc:title":"perovskite oxide"},{"@id":"https://cir.nii.ac.jp/all?q=synchrotron%20X-ray%20technique","dc:title":"synchrotron X-ray technique"},{"@id":"https://cir.nii.ac.jp/all?q=time-resolved%20measurement","dc:title":"time-resolved measurement"},{"@id":"https://cir.nii.ac.jp/all?q=topochemical%20reaction","dc:title":"topochemical reaction"}],"dcterms:subject":[{"subjectScheme":"Other","notation":[{"@language":"en","@value":"oxygen storage material"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"perovskite oxide"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"synchrotron X-ray technique"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"time-resolved measurement"}]},{"subjectScheme":"Other","notation":[{"@language":"en","@value":"topochemical reaction"}]}],"project":[{"@id":"https://cir.nii.ac.jp/crid/1040003825683128576","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"19K22230"},{"@type":"JGN","@value":"JP19K22230"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-19K22230/"}],"notation":[{"@language":"ja","@value":"圧縮率の違いを利用した層状化合物の創製"},{"@language":"en","@value":"Synthesis of layered compounds based on differences in compressibility"}]},{"@id":"https://cir.nii.ac.jp/crid/1040299826878925184","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"23K23035"},{"@type":"JGN","@value":"JP23K23035"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-23K23035/"}],"notation":[{"@language":"ja","@value":"特異なアニオン欠損面を持つ新規ペロブスカイトの開拓"},{"@language":"en","@value":"Investigation for novel perovskite compounds with unusual anion-deficient 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