{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1360002216613596032.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1021/acsami.5b05542"}},{"identifier":{"@type":"URI","@value":"https://pubs.acs.org/doi/pdf/10.1021/acsami.5b05542"}},{"identifier":{"@type":"PMID","@value":"26287811"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@value":"High-Concentration Synthesis of Sub-10-nm Copper Nanoparticles for Application to Conductive Nanoinks"}],"description":[{"notation":[{"@value":"A simple, high-concentration (up to 0.6 M Cu salt) synthesis of sub-10-nm copper nanoparticles (Cu NPs) was developed in ethylene glycol at room temperature under ambient air conditions using 1-amino-2-propanol (AmIP) as the stabilizer. Monodispersed AmIP-Cu NPs of 3.5 ± 1.0 nm were synthesized in a high yield of ∼90%. Thus, nearly 1 g of sub-10-nm Cu NP powder was obtained using a one-step synthesis for the first time. It is proposed that metallacyclic coordination stability of a five-membered ring type between the Cu and AmIP causes the high binding force of Am IP onto the Cu surface, resulting in the superior stability of the AmIP-Cu NPs in a solution. The purified powder of AmIP-Cu NPs can be redispersed in alcohol-based solvents up to high Cu contents of 45 wt % for the preparation of Cu nanoink. The resistivity of the conductive Cu film obtained from the Cu nanoink was 30 μΩ cm after thermal heating at 150 °C for 15 min under a nitrogen flow. The long-term resistance stability of the Cu film under an air atmosphere was also demonstrated."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1380284919776214529","@type":"Researcher","foaf:name":[{"@value":"Yuki Hokita"}],"jpcoar:affiliationName":[{"@value":"Faculty\rof Chemistry, Materials and Bioengineering, Kansai University, 3-3-35\rYamate-cho, Suita 564-8680, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380284919776214528","@type":"Researcher","foaf:name":[{"@value":"Mai Kanzaki"}],"jpcoar:affiliationName":[{"@value":"Faculty\rof Chemistry, Materials and Bioengineering, Kansai University, 3-3-35\rYamate-cho, Suita 564-8680, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380284919776214400","@type":"Researcher","foaf:name":[{"@value":"Tomonori Sugiyama"}],"jpcoar:affiliationName":[{"@value":"Faculty\rof Chemistry, Materials and Bioengineering, Kansai University, 3-3-35\rYamate-cho, Suita 564-8680, 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