{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1360004233240510592.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1021/la201550a"}},{"identifier":{"@type":"URI","@value":"https://pubs.acs.org/doi/pdf/10.1021/la201550a"}},{"identifier":{"@type":"PMID","@value":"21667918"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@value":"Non-surface Activity and Micellization Behavior of Cationic Amphiphilic Block Copolymer Synthesized by Reversible Addition–Fragmentation Chain Transfer Process"}],"description":[{"notation":[{"@value":"Cationic amphiphilic diblock copolymers of poly(n-butylacrylate)-b-poly(3-(methacryloylamino)propyl)trimethylammonium chloride) (PBA-b-PMAPTAC) with various hydrophobic and hydrophilic chain lengths were synthesized by a reversible addition-fragmentation chain transfer (RAFT) process. Their molecular characteristics such as surface activity/nonactivity were investigated by surface tension measurements and foam formation observation. Their micelle formation behavior and micelle structure were investigated by fluorescence probe technique, static and dynamic light scattering (SLS and DLS), etc., as a function of hydrophilic and hydrophobic chain lengths. The block copolymers were found to be non-surface active because the surface tension of the aqueous solutions did not change with increasing polymer concentration. Critical micelle concentration (cmc) of the polymers could be determined by fluorescence and SLS measurements, which means that these polymers form micelles in bulk solution, although they were non-surface active. Above the cmc, the large blue shift of the emission maximum of N-phenyl-1-naphthylamine (NPN) probe and the low micropolarity value of the pyrene probe in polymer solution indicate the core of the micelle is nonpolar in nature. Also, the high value of the relative intensity of the NPN probe and the fluorescence anisotropy of the 1,6-diphenyl-1,3,5-hexatriene (DPH) probe indicated that the core of the micelle is highly viscous in nature. DLS was used to measure the average hydrodynamic radii and size distribution of the copolymer micelles. The copolymer with the longest PBA block had the poorest water solubility and consequently formed micelles with larger size while having a lower cmc. The \"non-surface activity\" was confirmed for cationic amphiphilic diblock copolymers in addition to anionic ones studied previously, indicating the universality of non-surface activity nature."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1380004233240510592","@type":"Researcher","foaf:name":[{"@value":"Arjun Ghosh"}],"jpcoar:affiliationName":[{"@value":"Department of Polymer Chemistry, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380004233240510593","@type":"Researcher","foaf:name":[{"@value":"Shin-ichi Yusa"}],"jpcoar:affiliationName":[{"@value":"Graduate School of Engineering, University of Hyogo, 2167 Shosha, Himeji, Hyogo 671-2280, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380004233240510721","@type":"Researcher","foaf:name":[{"@value":"Hideki Matsuoka"}],"jpcoar:affiliationName":[{"@value":"Department of Polymer Chemistry, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380004233240510720","@type":"Researcher","foaf:name":[{"@value":"Yoshiyuki Saruwatari"}],"jpcoar:affiliationName":[{"@value":"Osaka Organic Chemical Industries Ltd., 7-20 Azuchi-Machi 1-Chome, Chuo-Ku, Osaka 541-0052, Japan"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"07437463"},{"@type":"EISSN","@value":"15205827"}],"prism:publicationName":[{"@value":"Langmuir"}],"dc:publisher":[{"@value":"American Chemical Society (ACS)"}],"prism:publicationDate":"2011-07-01","prism:volume":"27","prism:number":"15","prism:startingPage":"9237","prism:endingPage":"9244"},"reviewed":"false","url":[{"@id":"https://pubs.acs.org/doi/pdf/10.1021/la201550a"}],"createdAt":"2011-06-13","modifiedAt":"2024-04-07","project":[{"@id":"https://cir.nii.ac.jp/crid/1040000782110307968","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"22350106"},{"@type":"JGN","@value":"JP22350106"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-22350106/"}],"notation":[{"@language":"ja","@value":"光増感剤のフラーレン包接錯体を水に可溶化する 感温性ナノキャリアの開発"},{"@language":"en","@value":"Preparation of thermo-responsive nano-carrier which can solubilize fullerene complex as a photosensitizer in water"}]},{"@id":"https://cir.nii.ac.jp/crid/1040000782129248896","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"22655036"},{"@type":"JGN","@value":"JP22655036"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-22655036/"}],"notation":[{"@language":"ja","@value":"刺激応答性ピコリッターカップ配列体の創出"},{"@language":"en","@value":"Preparation of stimuli-responsive pico-liter cup array"}]},{"@id":"https://cir.nii.ac.jp/crid/1040000782140536576","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"23106717"},{"@type":"JGN","@value":"JP23106717"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PUBLICLY-23106717/"}],"notation":[{"@language":"ja","@value":"高度に機能化された感温性ソフトインターフェースを持つ架橋ポリマーソームの創成"}]},{"@id":"https://cir.nii.ac.jp/crid/1040282257004124672","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"20106006"},{"@type":"JGN","@value":"JP20106006"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PLANNED-20106006/"}],"notation":[{"@language":"ja","@value":"高分子イオン密生ソフト界面のナノ構造と機能の相関"},{"@language":"en","@value":"Nanostructure and Functionality of Polyelectrolyte Brush Soft Interface"}]},{"@id":"https://cir.nii.ac.jp/crid/1040282257463113728","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"10F00040"},{"@type":"JGN","@value":"JP10F00040"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-10F00040/"}],"notation":[{"@language":"ja","@value":"RAFTによる環境応答型イオン性両親媒性ブロックコポリマーの合成とその自己組織化"}]}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050564285769593856","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Sonication-induced formation of size-controlled self-assemblies of amphiphilic Janus-type polymers as optical tumor-imaging agents."},{"@value":"Sonication‐Induced Formation of Size‐Controlled Self‐Assemblies of Amphiphilic Janus‐Type Polymers as Optical Tumor‐Imaging Agents"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219111602432","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"Why Ionic Amphiphilic “<i>Block</i>” Copolymer Can Be Non-surface Active? 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