{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1360004233577137280.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1039/c3dt51696b"}},{"identifier":{"@type":"URI","@value":"http://pubs.rsc.org/en/content/articlepdf/2013/DT/C3DT51696B"}},{"identifier":{"@type":"PMID","@value":"23963158"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@value":"Metal array fabrication based on ultrasound-induced self-assembly of metalated dipeptides"}],"description":[{"notation":[{"@value":"Pd- and Pt-bound bis-metalated peptides were synthesised by the condensation of Pd- or Pt-aldimine-complex-bound glutamic acids to afford the four possible metal isomers of bis-Pd and bis-Pt-homometalated dipeptides and PdPt- and PtPd-heterometalated dipeptides without metal disproportionation. Ultrasound-induced self-assembly of these bis-metalated peptides proceeded effectively to afford supramolecular gels that displayed well-ordered metal arrays. The formation of parallel β-sheet type aggregates through interpeptide amide-amide hydrogen bonding was confirmed by IR, scanning electron microscopy (SEM), and synchrotron X-ray diffraction analyses (WAXS and SAXS). The mechanism of the ultrasound-induced self-assembly of the metalated dipeptides was elucidated via kinetic and association experiments by (1)H NMR, in which ultrasound-triggered dissociation of intramolecular hydrogen bonds between the chloride ligands of the Pd- and Pt-complexes and amides initially occurred. This was followed by the formation of intermolecular amide-amide hydrogen bonds, which afforded the corresponding oligomeric peptide self-assembly as the nucleus for supramolecular aggregation. The observed first-order relationship of the gelation rate versus the sonication frequency suggested that the microcavitation generated under sonication conditions acted as a crucial trigger and provided a reaction field for efficient self-assembly."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1380004233577137161","@type":"Researcher","foaf:name":[{"@value":"Katsuhiro Isozaki"}]},{"@id":"https://cir.nii.ac.jp/crid/1380004233577137411","@type":"Researcher","foaf:name":[{"@value":"Yusuke Haga"}]},{"@id":"https://cir.nii.ac.jp/crid/1380004233577137290","@type":"Researcher","foaf:name":[{"@value":"Kazuki Ogata"}]},{"@id":"https://cir.nii.ac.jp/crid/1030003658389059843","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"20164113"},{"@type":"NRID","@value":"1000020164113"},{"@type":"NRID","@value":"9000258595345"},{"@type":"NRID","@value":"9000399570930"},{"@type":"NRID","@value":"9000262347122"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/read0013723"}],"foaf:name":[{"@value":"Takeshi Naota"}]},{"@id":"https://cir.nii.ac.jp/crid/1380004233577137152","@type":"Researcher","foaf:name":[{"@value":"Hikaru Takaya"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"14779226"},{"@type":"EISSN","@value":"14779234"}],"prism:publicationName":[{"@value":"Dalton Transactions"}],"dc:publisher":[{"@value":"Royal Society of Chemistry (RSC)"}],"prism:publicationDate":"2013","prism:volume":"42","prism:number":"45","prism:startingPage":"15953"},"reviewed":"false","url":[{"@id":"http://pubs.rsc.org/en/content/articlepdf/2013/DT/C3DT51696B"}],"createdAt":"2013-07-25","modifiedAt":"2024-04-17","foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=Models,%20Molecular","dc:title":"Models, Molecular"},{"@id":"https://cir.nii.ac.jp/all?q=Glutamic%20Acid","dc:title":"Glutamic Acid"},{"@id":"https://cir.nii.ac.jp/all?q=Hydrogen%20Bonding","dc:title":"Hydrogen Bonding"},{"@id":"https://cir.nii.ac.jp/all?q=Dipeptides","dc:title":"Dipeptides"},{"@id":"https://cir.nii.ac.jp/all?q=Sonication","dc:title":"Sonication"},{"@id":"https://cir.nii.ac.jp/all?q=X-Ray%20Diffraction","dc:title":"X-Ray Diffraction"},{"@id":"https://cir.nii.ac.jp/all?q=Coordination%20Complexes","dc:title":"Coordination Complexes"},{"@id":"https://cir.nii.ac.jp/all?q=Scattering,%20Small%20Angle","dc:title":"Scattering, Small Angle"},{"@id":"https://cir.nii.ac.jp/all?q=Imines","dc:title":"Imines"},{"@id":"https://cir.nii.ac.jp/all?q=Gels","dc:title":"Gels"},{"@id":"https://cir.nii.ac.jp/all?q=Palladium","dc:title":"Palladium"},{"@id":"https://cir.nii.ac.jp/all?q=Platinum","dc:title":"Platinum"}],"project":[{"@id":"https://cir.nii.ac.jp/crid/1040000782197998976","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"24350070"},{"@type":"JGN","@value":"JP24350070"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-24350070/"}],"notation":[{"@language":"ja","@value":"渡環型白金錯体の集合分散制御に基づく高輝度リン光性物質の開拓"},{"@language":"en","@value":"Investigation of highly emissive platinum complexes bearing vaulted structure based on their aggregation control"}]},{"@id":"https://cir.nii.ac.jp/crid/1040000782266133760","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"25620059"},{"@type":"JGN","@value":"JP25620059"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-25620059/"}],"notation":[{"@language":"ja","@value":"有機金属分子のｄ－π共役制御に基づく角度可変汎用分子ジャンクションの構築"},{"@language":"en","@value":"Studies on transition metal complexes as a molecular junction with flexible coordination plane based on d-pai conjugation."}]},{"@id":"https://cir.nii.ac.jp/crid/1040282257166664704","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"24108719"},{"@type":"JGN","@value":"JP24108719"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PUBLICLY-24108719/"}],"notation":[{"@language":"ja","@value":"配位プログラミングによるメタル化ペプチド超構造体の創製と超分子触媒への展開"}]}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050282812513989504","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Organic solar cells. 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