{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1360021390766245120.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1063/5.0150091"}},{"identifier":{"@type":"URI","@value":"https://pubs.aip.org/aip/rsi/article-pdf/doi/10.1063/5.0150091/18103003/083103_1_5.0150091.pdf"}},{"identifier":{"@type":"PMID","@value":"38065179"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@value":"<i>In situ</i> high temperature powder x-ray diffraction technique using a sapphire single-crystal flat cell"}],"description":[{"type":"abstract","notation":[{"@value":"<jats:p>Understanding the behaviors of materials in their operating and manufacturing environments is essential not only in the scientific field, but also in the context of designing industrial materials for target applications. In this study, we developed a high-temperature x-ray diffraction (XRD) system, using a small microscope heating stage at the BL02B2 beamline in SPring-8. Newly designed sample cells composed of sapphire single crystals were employed to perform XRD experiments using powdered samples at high temperatures and under oxidization/reduction gas atmospheres, with a short sample exchange time. More specifically, XRD experiments were conducted under vacuum, air, inert gas (maximum temperature: ∼1400 °C), and reduction gas flow conditions (maximum temperature: ∼900 °C). In addition, to monitor the changes in the exhausted gas composition during the chemical reactions, the developed heating system was combined with in situ gas-analysis tools (a remote gas-pressure control system, gas chromatograph, and mass spectrometer), which allowed analysis of the gas-adsorption/desorption and solid–gas reaction processes. Several heating experiments, such as the observation of the reduction of Fe oxides, phase transitions of ZrO2 and BaCO3, and synthesis of BaZrO3, demonstrated the validity and usefulness of this system.</jats:p>"}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1380021390766245121","@type":"Researcher","foaf:name":[{"@value":"S. Kobayashi"}],"jpcoar:affiliationName":[{"@value":"Japan Synchrotron Radiation Research Institute , Sayo, Hyogo, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380021390766245120","@type":"Researcher","foaf:name":[{"@value":"S. Kawaguchi"}],"jpcoar:affiliationName":[{"@value":"Japan Synchrotron Radiation Research Institute , Sayo, Hyogo, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1380021390766245249","@type":"Researcher","foaf:name":[{"@value":"H. Yamada"}],"jpcoar:affiliationName":[{"@value":"Japan Synchrotron Radiation Research Institute , Sayo, Hyogo, Japan"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"00346748"},{"@type":"EISSN","@value":"10897623"}],"prism:publicationName":[{"@value":"Review of Scientific Instruments"}],"dc:publisher":[{"@value":"AIP Publishing"}],"prism:publicationDate":"2023-08-01","prism:volume":"94","prism:number":"8","prism:startingPage":"083103"},"reviewed":"false","url":[{"@id":"https://pubs.aip.org/aip/rsi/article-pdf/doi/10.1063/5.0150091/18103003/083103_1_5.0150091.pdf"}],"createdAt":"2023-08-28","modifiedAt":"2023-08-29","project":[{"@id":"https://cir.nii.ac.jp/crid/1040018351904921984","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"23K28362"},{"@type":"JGN","@value":"JP23K28362"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-23K28362/"}],"notation":[{"@language":"ja","@value":"不可逆ガス吸着過程をターゲットにしたミリ秒高精度粉末回折手法の開発"}]},{"@id":"https://cir.nii.ac.jp/crid/1040854882542342784","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"22K14487"},{"@type":"JGN","@value":"JP22K14487"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-22K14487/"}],"notation":[{"@language":"ja","@value":"高温合成過程のその場観測のための透過型高エネルギーX線構造解析システムの確立"},{"@language":"en","@value":"Development of a high-energy transmission X-ray diffraction system for in situ observation of high temperature synthesis processes"}]}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050001202626562560","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"en","@value":"High-throughput powder diffraction measurement system consisting of multiple MYTHEN detectors at beamline BL02B2 of SPring-8"}]},{"@id":"https://cir.nii.ac.jp/crid/1360011143576565248","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Reduction of Fe2O3 with hydrogen"}]},{"@id":"https://cir.nii.ac.jp/crid/1360011143673383168","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"New cements for the 21st century: The pursuit of an alternative to Portland 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