{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1360285708442564352.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1038/s41467-017-02250-4"}},{"identifier":{"@type":"URI","@value":"https://www.nature.com/articles/s41467-017-02250-4.pdf"}},{"identifier":{"@type":"URI","@value":"https://www.nature.com/articles/s41467-017-02250-4"}}],"resourceType":"学術雑誌論文(journal article)","dc:title":[{"@value":"Solution-phase synthesis of Al13\n                     − using a dendrimer template"}],"description":[{"type":"abstract","notation":[{"@value":"<jats:title>Abstract</jats:title><jats:p>Superatoms, clusters that mimic the properties of elements different to those of which they are composed, have the potential to serve as building blocks for unprecedented materials with tunable properties. The development of a method for the solution-phase synthesis of superatoms would be an indispensable achievement for the future progress of this research field. Here we report the fabrication of aluminum clusters in solution using a dendrimer template, producing Al<jats:sub>13</jats:sub><jats:sup>−</jats:sup>, which is the most well-known superatom. The Al<jats:sub>13</jats:sub><jats:sup>−</jats:sup> cluster is identified using mass spectrometry and scanning transmission electron microscopy, and X-ray photoelectron spectroscopy is used to measure the binding energies. The superatomic stability of Al<jats:sub>13</jats:sub><jats:sup>−</jats:sup> is demonstrated by evaluating its tendency toward oxidation. In addition, the synthesis of Al<jats:sub>13</jats:sub><jats:sup>−</jats:sup> in solution enables electrochemical measurements, the results of which suggest oxidation of Al<jats:sub>13</jats:sub><jats:sup>−</jats:sup>. This solution-phase synthesis of Al<jats:sub>13</jats:sub><jats:sup>−</jats:sup> superatoms has a significant role for the experimental development of cluster science.</jats:p>"}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1420564276158845952","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"00733495"},{"@type":"NRID","@value":"1000000733495"},{"@type":"NRID","@value":"9000413750862"},{"@type":"NRID","@value":"9000398144440"},{"@type":"NRID","@value":"9000390928778"},{"@type":"NRID","@value":"9000242087417"},{"@type":"NRID","@value":"9000283393581"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/kambe"}],"foaf:name":[{"@value":"Tetsuya Kambe"}]},{"@id":"https://cir.nii.ac.jp/crid/1380285708442564225","@type":"Researcher","foaf:name":[{"@value":"Naoki Haruta"}]},{"@id":"https://cir.nii.ac.jp/crid/1380285708442564489","@type":"Researcher","foaf:name":[{"@value":"Takane Imaoka"}]},{"@id":"https://cir.nii.ac.jp/crid/1420845751165872896","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"80220458"},{"@type":"NRID","@value":"1000080220458"},{"@type":"ORCID","@value":"0000-0001-7851-0519"},{"@type":"NRID","@value":"9000019191636"},{"@type":"NRID","@value":"9000375849401"},{"@type":"NRID","@value":"9000404540624"},{"@type":"NRID","@value":"9000000116020"},{"@type":"NRID","@value":"9000347106612"},{"@type":"NRID","@value":"9000256045319"},{"@type":"NRID","@value":"9000001189217"},{"@type":"NRID","@value":"9000297506476"},{"@type":"NRID","@value":"9000345264455"},{"@type":"NRID","@value":"9000399794898"},{"@type":"NRID","@value":"9000413949355"},{"@type":"NRID","@value":"9000398144443"},{"@type":"NRID","@value":"9000390928779"},{"@type":"NRID","@value":"9000370759020"},{"@type":"NRID","@value":"9000402492266"},{"@type":"NRID","@value":"9000009903002"},{"@type":"NRID","@value":"9000347163403"}],"foaf:name":[{"@value":"Kimihisa Yamamoto"}]}],"publication":{"publicationIdentifier":[{"@type":"EISSN","@value":"20411723"}],"prism:publicationName":[{"@value":"Nature Communications"}],"dc:publisher":[{"@value":"Springer Science and Business Media LLC"}],"prism:publicationDate":"2017-12-11","prism:volume":"8","prism:number":"1","prism:startingPage":"2046"},"reviewed":"false","dcterms:accessRights":"http://purl.org/coar/access_right/c_abf2","dc:rights":["https://creativecommons.org/licenses/by/4.0","https://creativecommons.org/licenses/by/4.0"],"url":[{"@id":"https://www.nature.com/articles/s41467-017-02250-4.pdf"},{"@id":"https://www.nature.com/articles/s41467-017-02250-4"}],"createdAt":"2017-12-05","modifiedAt":"2022-12-22","foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=Science","dc:title":"Science"},{"@id":"https://cir.nii.ac.jp/all?q=Q","dc:title":"Q"},{"@id":"https://cir.nii.ac.jp/all?q=Article","dc:title":"Article"}],"project":[{"@id":"https://cir.nii.ac.jp/crid/1040000781965902976","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"17K05804"},{"@type":"JGN","@value":"JP17K05804"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-17K05804/"}],"notation":[{"@language":"ja","@value":"鋳型デンドリマーを用いた典型金属クラスターの精密合成と超原子機能の開拓"},{"@language":"en","@value":"Investigation of superatomic functionality through precisely controlled synthesis of typical metal cluster using dendrimer templates"}]},{"@id":"https://cir.nii.ac.jp/crid/1040000782440002560","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"15H05757"},{"@type":"JGN","@value":"JP15H05757"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-15H05757/"}],"notation":[{"@language":"ja","@value":"精密無機合成を基盤とする超原子の創成と機能解明"},{"@language":"en","@value":"Creation of Superatoms Based on the Precision Inorganic Synthesis and Elucidation of its Function"}]}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1360002216618539136","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Precision Synthesis of Subnanoparticles Using Dendrimers as a Superatom Synthesizer"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219111724160","@type":"Article","resourceType":"学術雑誌論文(journal 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cluster beams"}]},{"@id":"https://cir.nii.ac.jp/crid/1363951794458509696","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Electric response properties of neutral and charged Al13X (X=Li, Na, K) magic clusters. A comprehensive ab initio and density functional comparative study"}]},{"@id":"https://cir.nii.ac.jp/crid/1363951795675720448","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Structures of Aln, its anions and cations up to n=34: A theoretical investigation"}]},{"@id":"https://cir.nii.ac.jp/crid/1363951796148092544","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"A Systematic Framework and Nanoperiodic Concept for Unifying Nanoscience: Hard/Soft Nanoelements, Superatoms, Meta-Atoms, New Emerging Properties, Periodic Property Patterns, and Predictive Mendeleev-like Nanoperiodic Tables"}]},{"@id":"https://cir.nii.ac.jp/crid/1364233270597384704","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Superatom Compounds, Clusters, and Assemblies:  Ultra Alkali Motifs and 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