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Here we report on how the intimate coupling of synthesis, in-depth electron tomographic characterization and theory enables exquisite control of superstructure in highly ordered porous three-dimensional continuous networks from single and binary mixtures of metal nanoparticles with a triblock terpolymer. Poly(isoprene-block-styrene-block-(N,N-dimethylamino)ethyl methacrylate) is synthesized and used as structure-directing agent for ligand-stabilized platinum and gold nanoparticles. Quantitative analysis provides insights into short- and long-range nanoparticle-nanoparticle correlations, and local and global contributions to structural chirality in the networks. Results provide synthesis criteria for next-generation mesoporous network superstructures from binary nanoparticle mixtures for potential applications in areas including catalysis."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1380003444993492230","@type":"Researcher","foaf:name":[{"@value":"Zihui Li"}]},{"@id":"https://cir.nii.ac.jp/crid/1380003444993492225","@type":"Researcher","foaf:name":[{"@value":"Kahyun Hur"}]},{"@id":"https://cir.nii.ac.jp/crid/1380003444993492227","@type":"Researcher","foaf:name":[{"@value":"Hiroaki 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iroshi 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Gruner"}]},{"@id":"https://cir.nii.ac.jp/crid/1380003444993492231","@type":"Researcher","foaf:name":[{"@value":"Ulrich Wiesner"}]}],"contributor":[{"@id":"https://cir.nii.ac.jp/crid/1893118015420444167","@type":"Researcher","foaf:name":[{"@value":"Cornell University, Ithaca, United States"}]},{"@id":"https://cir.nii.ac.jp/crid/1893118015420444163","@type":"Researcher","foaf:name":[{"@value":"Kyushu University, Fukuoka, Japan"}]}],"publication":{"publicationIdentifier":[{"@type":"EISSN","@value":"20411723"}],"prism:publicationName":[{"@value":"Nature Communications"}],"dc:publisher":[{"@value":"Springer Science and Business Media 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Acids"},{"@id":"https://cir.nii.ac.jp/all?q=Nanoparticles","dc:title":"Nanoparticles"},{"@id":"https://cir.nii.ac.jp/all?q=Polystyrenes","dc:title":"Polystyrenes"},{"@id":"https://cir.nii.ac.jp/all?q=Gold","dc:title":"Gold"},{"@id":"https://cir.nii.ac.jp/all?q=Platinum","dc:title":"Platinum"}],"project":[{"@id":"https://cir.nii.ac.jp/crid/1040282257172611840","@type":"Project","projectIdentifier":[{"@type":"KAKEN","@value":"24310092"},{"@type":"JGN","@value":"JP24310092"},{"@type":"URI","@value":"https://kaken.nii.ac.jp/grant/KAKENHI-PROJECT-24310092/"}],"notation":[{"@language":"ja","@value":"メゾらせんハイブリッド構造の創成とその機能"},{"@language":"en","@value":"Development of meso-scale chiral nano-composite based on self-assembly of an ABC block copolymer"}]}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050306506453119872","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Electrochemical synthesis 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