Precise determination of iridium by neutron activation analysis coupled with internal standard method

Bibliographic Information

Published
2020-04-16
Resource Type
journal article
Rights Information
  • https://www.springer.com/tdm
  • https://www.springer.com/tdm
DOI
  • 10.1007/s10967-020-07152-2
Publisher
Springer Science and Business Media LLC

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Description

Instrumental neutron activation analysis with internal standard correction was applied for precise determine of mg quantities of Ir in high-purity IrBr4. A known amount of Au standard solution was used as an internal standard to compensate for inhomogeneity of the neutron flux through an irradiation capsule and for neutron self-shielding. The linearity of the calibration curves of Ir was improved by using an internal standard. The relative expanded uncertainty (k = 2) associated with the determined value was 0.86%, which allowed the mg quantities of iridium to be precisely determined.

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