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Although Raman‐based barometry is an effective method for ascertaining the internal pressure of H<jats:sub>2</jats:sub>O–CO<jats:sub>2</jats:sub> fluid inclusions, few studies have elucidated Raman spectral features of CO<jats:sub>2</jats:sub> in a system of high‐pressure H<jats:sub>2</jats:sub>O–CO<jats:sub>2</jats:sub>. New experiments using a high‐pressure optical cell in this binary system with compositions of 100, 75 ± 2, and 60 ± 2 mol% CO<jats:sub>2</jats:sub> were conducted for this study to verify the availability of Raman CO<jats:sub>2</jats:sub> barometers for use in assessing the temperature and pressure conditions of approximately 22°C and 17.3–141.4 MPa. Our results demonstrate that the existence of H<jats:sub>2</jats:sub>O does not affect the relation between Fermi diad splits (Δ, cm<jats:sup>−1</jats:sup>) and total pressure of pure CO<jats:sub>2</jats:sub>. These results suggest that the Δ–total pressure relation obtained from pure CO<jats:sub>2</jats:sub> is also applicable to H<jats:sub>2</jats:sub>O–CO<jats:sub>2</jats:sub> systems, even at high pressure. However, unlike Δ, because the peak positions of the Fermi diad in the system of H<jats:sub>2</jats:sub>O–CO<jats:sub>2</jats:sub> shift to a higher wavenumber than those of pure CO<jats:sub>2</jats:sub> at given pressure higher than 30 MPa, the peak positions are not very suitable for the pressure scale in an H<jats:sub>2</jats:sub>O–CO<jats:sub>2</jats:sub> system. Additionally, we confirmed the availability of bandwidths of CO<jats:sub>2</jats:sub> as an indicator of compositions that can identify the presence of very small amounts of H<jats:sub>2</jats:sub>O (at least 0.3 mol% H<jats:sub>2</jats:sub>O), even at room temperature.</jats:p>"}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1381412889656232832","@type":"Researcher","foaf:name":[{"@value":"Yuuki Hagiwara"}],"jpcoar:affiliationName":[{"@value":"Graduate School of Science Hokkaido University  Sapporo Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1381412889656232704","@type":"Researcher","foaf:name":[{"@value":"Junji Torimoto"}],"jpcoar:affiliationName":[{"@value":"Ore Genesis Research Unit, Project Team for Development of New‐Generation Research Protocol for Submarine Resources JAMSTEC  Yokosuka‐shi 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