{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1362825895909092608.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1063/1.1743184"}},{"identifier":{"@type":"URI","@value":"https://pubs.aip.org/aip/jcp/article-pdf/25/6/1228/18811441/1228_1_online.pdf"}},{"identifier":{"@type":"NAID","@value":"30015712174"}}],"dc:title":[{"@value":"Rate Processes and Nuclear Magnetic Resonance Spectra. II. Hindered Internal Rotation of Amides"}],"description":[{"type":"abstract","notation":[{"@value":"<jats:p>Mathematical methods are presented for calculating rate constants of processes which narrow nuclear magnetic resonance absorption lines having discrete components. High resolution proton spectra show that the R1CO-NR2R3 skeletons of N,N-dimethylformamide (DMF) and N,N-dimethylacetamide (DMA) are planar and suggest that N-methylformamide, N-methylacetamide, N-methylformanilide and N-methylacetanilide exist predominantly in one configuration. The presence of a significant amount of double bond character in the C–N amide bond is proved by the temperature dependent coalescence observed for the chemically shifted proton doublet of the N(CH3)2 groups in DMF and DMA, which gives values of about 22 and 19 kcal respectively for the free energy of activation required for reorientations about the bond.</jats:p>"}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1581698598986607744","@type":"Researcher","foaf:name":[{"@value":"H. S. Gutowsky"}],"jpcoar:affiliationName":[{"@value":"Noyes Chemical Laboratory, University of Illinois, Urbana, Illinois"}]},{"@id":"https://cir.nii.ac.jp/crid/1382825895909092609","@type":"Researcher","foaf:name":[{"@value":"C. H. Holm"}],"jpcoar:affiliationName":[{"@value":"Noyes Chemical Laboratory, University of Illinois, Urbana, Illinois"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"00219606"},{"@type":"EISSN","@value":"10897690"}],"prism:publicationName":[{"@value":"The Journal of Chemical Physics"}],"dc:publisher":[{"@value":"AIP Publishing"}],"prism:publicationDate":"1956-12-01","prism:volume":"25","prism:number":"6","prism:startingPage":"1228","prism:endingPage":"1234"},"reviewed":"false","url":[{"@id":"https://pubs.aip.org/aip/jcp/article-pdf/25/6/1228/18811441/1228_1_online.pdf"}],"createdAt":"2005-01-06","modifiedAt":"2024-02-08","relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1360002219098796544","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"Electron Spin Resonance of X-Irradiated Single Crystals of Zinc Acetate Dihydrate: Hindered Rotation of Methylene Group in a Free Radical CH2COO−"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219098839808","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"The Effect of Hydrogen Bonding on the Rates of Inversion of 1-Hydroxy-5, 7-dihydrodibenz[<i>c</i>,<i>e</i>]oxepin"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219099851008","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"The Triplet Excitons in the Anion Radical Salts of [(C6H5)3PCH3]1−<i>x</i>+[(C6H5)3AsCH3]<i>x</i>+ (TCNQ)2÷, (0≤<i>x</i>≤1)"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219102566784","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"Conformational Changes of 1,2,3-Triselena- and 1,2,3-Trithia[3]( 1,1′)ruthenocenophane"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219103424000","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"Hindered Internal Rotation Around the C–N Bond in 1<i>H</i>-Azepine Derivatives as Studied by the NMR Techniques"}]},{"@id":"https://cir.nii.ac.jp/crid/1360002219106357376","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@value":"LAYERED COMPOUNDS. 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