{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1363670318517499008.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1021/ma051232r"}},{"identifier":{"@type":"URI","@value":"https://pubs.acs.org/doi/pdf/10.1021/ma051232r"}}],"dc:title":[{"@value":"Crystal Modifications and Thermal Behavior of Poly(<scp>l</scp>-lactic acid) Revealed by Infrared Spectroscopy"}],"description":[{"notation":[{"@value":"Recently, we reported the isothermal crystallization behaviors of poly(l-lactic acid) (PLLA) from the melt and glassy states, respectively [J. Phys. Chem. B 2004, 108, 11514; Macromolecules 2004, 37, 6433]. Surprisingly, the quite different infrared (IR) spectral evolutions occur in the two crystallization processes at different temperatures in which the same crystal modification is expected to be formed. To clarify this unusual phenomenon, the crystal modifications and thermal behavior of PLLA samples prepared under different crystallization temperatures are investigated in detail by TEM, WAXD, and FTIR techniques. On the basis of the WAXD and IR data, a new crystal modification named the α form is proposed for the crystal structure of PLLA samples annealed at temperature below 120 °C. Such crystal modification with loose 103 helical chain packing is less thermally stable than the standard α form of PLLA. This assignment can explain all the experiment observations well. Other possible mechanisms for the ..."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1383670318517499008","@type":"Researcher","foaf:name":[{"@value":"Jianming Zhang"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]},{"@id":"https://cir.nii.ac.jp/crid/1383670318517499009","@type":"Researcher","foaf:name":[{"@value":"Yongxin Duan"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]},{"@id":"https://cir.nii.ac.jp/crid/1383670318517499010","@type":"Researcher","foaf:name":[{"@value":"Harumi Sato"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]},{"@id":"https://cir.nii.ac.jp/crid/1383670318517499012","@type":"Researcher","foaf:name":[{"@value":"Hideto Tsuji"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]},{"@id":"https://cir.nii.ac.jp/crid/1383670318517499011","@type":"Researcher","foaf:name":[{"@value":"Isao Noda"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]},{"@id":"https://cir.nii.ac.jp/crid/1383670318517499013","@type":"Researcher","foaf:name":[{"@value":"Shouke Yan"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]},{"@id":"https://cir.nii.ac.jp/crid/1383670318517499014","@type":"Researcher","foaf:name":[{"@value":"Yukihiro Ozaki"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, School of Science and Technology, and Research Center for Environment Friendly Polymers, Kwansei-Gakuin University, Gakuen, Sanda 669-1337, Japan; Department of Ecological Engineering, Faculty of Engineering, Toyohashi University of Technology, Tempaku-cho, Toyohashi, Aichi 441-8580, Japan; State Key Laboratory of Polymer Physics & Chemistry, Institute of Chemistry, Chinese Academy of Sciences, Beijing 100080, P. R. China; and The Procter & Gamble Company, 8611 Beckett Road, West..."}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"00249297"},{"@type":"EISSN","@value":"15205835"}],"prism:publicationName":[{"@value":"Macromolecules"}],"dc:publisher":[{"@value":"American Chemical Society (ACS)"}],"prism:publicationDate":"2005-08-20","prism:volume":"38","prism:number":"19","prism:startingPage":"8012","prism:endingPage":"8021"},"reviewed":"false","url":[{"@id":"https://pubs.acs.org/doi/pdf/10.1021/ma051232r"}],"createdAt":"2005-09-13","modifiedAt":"2023-03-08","relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050564288865380224","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Biomass-Based Composites from Poly(lactic acid) and Wood Flour by Vapor-Phase Assisted Surface 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Structures and Controlling Their Physical Properties"},{"@language":"ja-Kana","@value":"センイジョウ オヨビ キュウジョウ コウゾウ ノ コウチク ニ ヨル コウブンシ ゲル ノ サクセイ ト ブッセイ セイギョ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282681502193792","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"New Developments in the Simultaneous Measurement System of Wide-Angle and Small-Angle X-ray Scatterings and Vibrational Spectra for the Static and Dynamic Analyses of the Hierarchical Structures of Polymer Solids"},{"@language":"ja","@value":"高分子階層構造の静的・動的解析のための広角小角X線散乱/振動スペクトル同時測定システムの開発と展開"},{"@value":"Development of simultaneous measurement system of wide- and small-angle X-ray scattering and vibrational spectra for the static and dynamic analyses of hierarchical structures of 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