{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1364233269182811136.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1021/ja905368d"}},{"identifier":{"@type":"URI","@value":"https://pubs.acs.org/doi/pdf/10.1021/ja905368d"}},{"identifier":{"@type":"PMID","@value":"19715318"}},{"identifier":{"@type":"HANDLE","@value":"2433/109713"}}],"dc:title":[{"@value":"Oxalate-Bridged Bimetallic Complexes {NH(prol)<sub>3</sub>}[MCr(ox)<sub>3</sub>] (M = Mn<sup>II</sup>, Fe<sup>II</sup>, Co<sup>II</sup>; NH(prol)<sub>3</sub><sup>+</sup> = Tri(3-hydroxypropyl)ammonium) Exhibiting Coexistent Ferromagnetism and Proton Conduction"}],"description":[{"notation":[{"@value":"The oxalate-bridged bimetallic complexes {NH(prol)(3)}[M(II)Cr(III)(ox)(3)] (M(II) = Mn(II), Fe(II), Co(II)) with hydrophilic tri(3-hydroxypropyl)ammonium (NH(prol)(3)(+)) were prepared by a new synthetic procedure, and the effects of the NH(prol)(3)(+) ion upon the structure, magnetism, and electrical conduction were studied. An X-ray crystallographic study of the MnCr dihydrate, {NH(prol)(3)}[MnCr(ox)(3)].2H(2)O, was performed. Crystal data: hexagonal, P6(3), a = b = 9.3808(14) A, c = 15.8006(14) A, Z = 2. The structure comprises oxalate-bridged bimetallic layers interleaved by NH(prol)(3)(+) ions. The ions assume a tripodal configuration and are hydrogen bonded to the bimetallic layers together with water molecules, giving rise to a short interlayer separation (7.90 A) and unsymmetrical faces to the bimetallic layer. Cryomagnetic studies demonstrate ferromagnetic ordering with transition temperature of 5.5 K for the MnCr complex, 9.0 K for the FeCr complex, and 10.0 K for the CoCr complex. The interlayer magnetic interaction is negligibly weak in all of the complexes despite the short interlayer separation. A slow magnetization is observed in all the complexes. This is explained by spin canting associated with the unsymmetrical feature of the bimetallic layer. The complexes show proton conduction of 1.2 x 10(-10) to 4.4 x 10(-10) S cm(-1) under 40% relative humidity (RH) and approximately 1 x 10(-4) S cm(-1) under 75% RH. On the basis of water adsorption/desorption profiles, the conduction under 40% RH is mediated through the hydrogen-bonded network formed by the bimetallic layer, NH(prol)(3)(+) ions, and water molecules (two per MCr). Under 75% RH, additional water molecules (three per MCr) are concerned with the high proton conduction. This is the first example of a metal complex system exhibiting coexistent ferromagnetism and proton conduction."}]}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1384233269182811266","@type":"Researcher","foaf:name":[{"@value":"Hisashi O̅kawa"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1384233269182811136","@type":"Researcher","foaf:name":[{"@value":"Akihito Shigematsu"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1384233269182811264","@type":"Researcher","foaf:name":[{"@value":"Masaaki Sadakiyo"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1384233269182811137","@type":"Researcher","foaf:name":[{"@value":"Takuya Miyagawa"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1384233269182811265","@type":"Researcher","foaf:name":[{"@value":"Ko Yoneda"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1384233269182811139","@type":"Researcher","foaf:name":[{"@value":"Masaaki Ohba"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1384233269182811138","@type":"Researcher","foaf:name":[{"@value":"Hiroshi Kitagawa"}],"jpcoar:affiliationName":[{"@value":"Department of Chemistry, Faculty of Science, Kyushu University, Hakozaki 8-10-1, Higashi-ku, Fukuoka 812-8581, Japan, Department of Synthetic Chemistry and Biological Chemistry, Graduate School of Engineering, Kyoto University, Katsura, Nishikyo-ku, Kyoto 615-8510, Japan, and JST-CREST, Sanban-cho 5, Chiyoda-ku, Tokyo 102-0075, Japan"}]}],"contributor":[{"@id":"https://cir.nii.ac.jp/crid/1890584741040697728","@type":"Researcher","foaf:name":[{"@value":"90234244"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"00027863"},{"@type":"EISSN","@value":"15205126"}],"prism:publicationName":[{"@value":"Journal of the American Chemical Society"}],"dc:publisher":[{"@value":"American Chemical Society (ACS)"}],"prism:publicationDate":"2009-08-28","prism:volume":"131","prism:number":"37","prism:startingPage":"13516","prism:endingPage":"13522"},"reviewed":"false","url":[{"@id":"https://pubs.acs.org/doi/pdf/10.1021/ja905368d"}],"createdAt":"2009-08-28","modifiedAt":"2023-03-13","relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050001335838221184","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"A significant change in selective adsorption behaviour for ethanol by flexibility control through the type of central metals in a metal-organic framework"}]},{"@id":"https://cir.nii.ac.jp/crid/1050297836158059136","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Control of Proton‐Conductive Behavior with Nanoenvironment within Metal–Organic Materials"},{"@value":"Control of proton-conductive behavior with 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