P15 ソノケミカル反応によるカーボンナノ粒子の合成(物質創製、他)

DOI

書誌事項

タイトル別名
  • P15 Sonochemical Synthesis of Carbon Nanoparticles(Materials Synthesis, etc.)
公開日
2003
DOI
  • 10.20577/pamjss.12.0_99
公開者
日本ソノケミストリー学会

説明

Sonochemical polymerization induced by applying ultrasound to benzene derivatives has been studied. Irradiating ultrasound to o-dichlorobenzene with solid particles such as zinc, its chloride, or nitrate produced various nanoparticles. In the case of using zinc nitrate, solid needle-like particles were obtained, when zinc metal and zinc nitrate were co-doped, hollow needle-like (tubular) particles were obtained. It is bound from the diffraction pattern that tubular particle has a polycrystalline structure, which could not be identified up to now. EDS analysis showed that the tubular particle contained Zinc element. When the particles were produced, Zinc element might be attracted inside or outside of the tubular particle. Various irradiation time and content of solid particles were tried, there might exist optimum parameter that increase a ratio of tubular particles respectively. In this research, the best parameter of the synthesis was; Irradiation time = 5 minutes Zinc: Zinc nitrate = 0.37wt%: 0.37wt% for o-dichlorobenzene.

収録刊行物

詳細情報 詳細情報について

  • CRID
    1390001206051343872
  • NII論文ID
    110009710233
  • DOI
    10.20577/pamjss.12.0_99
  • ISSN
    24241512
  • 本文言語コード
    ja
  • データソース種別
    • JaLC
    • CiNii Articles
  • 抄録ライセンスフラグ
    使用不可

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