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Improvement of the Direct Determination Method of Linamarin in Beans and Bean Paste Products
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- KAWAMURA Yoko
- National Institute of Hygienic Sciences
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- HIKIDI Siga
- Showa University
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- MARUYAMA Kouji
- Central Research Laboratory, Japan Grain Inspection Association
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- UCHIYAMA Sadao
- National Institute of Hygienic Sciences
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- SAITO Yukio
- National Institute of Hygienic Sciences
Bibliographic Information
- Other Title
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- 雑豆及びあん製品中のリナマリンの改良直接分析法
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Description
A method for the direct determination of linamarin, a cyanogenic glycoside in beans, bean paste products and cassava flour was improved. A sample was extracted with a mixture of acetonitrile and water, cleaned up by using a solid-phase extraction cartridge, and trimethylsilylated, then linamarin was quantitated by FID-GC and confirmed by GC/MS. The detection limit of linamarin was 1μg/g in beans, 0.25μg/g in dry bean paste and 0.1μg/g in raw paste. The contents of linamarin in beans, bean paste products and cassava flour were surveyed. The contents of linamarin determined by the proposed method were in good accordance with those found by the headspace GC method.
Journal
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- Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi)
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Food Hygiene and Safety Science (Shokuhin Eiseigaku Zasshi) 34 (1), 74-79_1, 1993
Japanese Society for Food Hygiene and Safety
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Keywords
Details 詳細情報について
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- CRID
- 1390282679203740672
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- NII Article ID
- 130003693171
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- COI
- 1:CAS:528:DyaK3sXitFWms74%3D
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- ISSN
- 18821006
- 00156426
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- Data Source
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- JaLC
- Crossref
- CiNii Articles
- OpenAIRE
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- Abstract License Flag
- Disallowed