Evaluation of a High-resolution Gas Chromatography/High-resolution Mass Spectrometry Method for the Determination of Dioxin and Related Compounds.

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  • ダイオキシンおよび関連化合物質のＨＲＧＣ／ＨＲＭＳによる超微量分離定量分析における最適条件化の検討

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Dioxin analysis requires high sensitivity, high selectivity and specificity. Currently, the analytical method of choice is high-resolution gas chromatography/high-resolution mass spectrometry (HRGC/HRMS) using the SIM method after extensive clean-up.<BR>In this paper, relative efficiencies and performances of both of various sample clean-up methods and HRGC/HRMS method were investigated and evaluated in detail. Some of the noteworthy problems were pointed out and discussed, and the most suitable combination of the procedures for Dioxin analysis were suggested.

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