{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1390282679489953024.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1252/kakoronbunshu.36.201"}},{"identifier":{"@type":"COI","@value":"1:CAS:528:DC%2BC3cXht1KitLfI"}},{"identifier":{"@type":"NDL_BIB_ID","@value":"10784734"}},{"identifier":{"@type":"URI","@value":"http://id.ndl.go.jp/bib/10784734"}},{"identifier":{"@type":"URI","@value":"https://ndlsearch.ndl.go.jp/books/R000000004-I10784734"}},{"identifier":{"@type":"URI","@value":"http://www.jstage.jst.go.jp/article/kakoronbunshu/36/4/36_4_201/_pdf"}},{"identifier":{"@type":"NAID","@value":"10027040534"}}],"dc:title":[{"@language":"en","@value":"Nickel Recycling from Spent Electroless Nickel Plating Baths Using Solvent Extraction"},{"@language":"ja","@value":"溶媒抽出法を用いた使用済み無電解ニッケルめっき液からのニッケルリサイクルに関する研究"},{"@language":"ja-Kana","@value":"ヨウバイ チュウシュツホウ オ モチイタ シヨウズミ ムデンカイ ニッケルメッキ エキ カラ ノ ニッケルリサイクル ニ カンスル ケンキュウ"}],"dc:language":"ja","description":[{"type":"abstract","notation":[{"@language":"en","@value":"Demand is growing for the recovery of nickel from spent electroless nickel plating baths (spent bath). The present authors have been studying the application of solvent extraction to this problem, and their findings are outlined in this review. On the basis of batch extraction experiments, a recycling process was established consisting of two steps: (i) impurity removal, followed by (ii) nickel recovery. In step (i), iron and zinc as impurities in the spent baths are selectively removed using acidic organophosphorous reagent such as PC88A. In step (ii), after increasing the pH to around 6, nickel in the spent baths is extracted using the chelating reagent LIX84I as an extractant aided by a small amount of PC88A as an accelerator. The nickel in the organic phase formed is stripped with 1–2 mol/dm<sup>3</sup> of sulfuric acid in order to obtain nickel sulfate solution, which is reused in the plating process. After the nickel extraction step had been validated by the continuous multistage experiment, in which high efficiencies were obtained during the extraction and stripping, this process was introduced in a plating plant and has been stably operated for more than one year. The bath life extension gained by removing impurities or byproducts using solvent extraction was also studied. Zinc in the strike nickel plating bath used for plating on an aluminum surface treated with zincate solution was found to be selectively removed using acidic organophosphorous reagent. This zinc removal process was installed in the plating plant and succeeded in extending the life of the strike bath by 3–5 times."},{"@language":"ja","@value":"使用済みの無電解ニッケルめっき液（使用済み液）からニッケルを回収しリサイクルする技術が求められている．本稿では，筆者らが研究してきた，溶媒抽出法を適用した技術を紹介する．バッチ実験の結果に基づき，まず酸性有機リン抽出剤であるPC88Aを用いて使用済み液中の不純物である鉄や亜鉛を選択的に除去し，その後pHを6付近に上げて，キレート試薬であるLIX84Iに少量のPC88Aを加速剤とした有機相を用いてニッケルを抽出し，得られる有機相を1–2 mol/dm<sup>3</sup>の硫酸で逆抽出することにより，ニッケルを硫酸ニッケル溶液として回収し，めっき工程で再使用するプロセスを開発した．向流多段操作の実験も行い，高効率でニッケルを回収できることを確認し，めっき工場において実用に供することができた．まためっき液中の不純物や副生成物を除去することによるめっき液長寿命化の研究も併せて行ったところ，アルミ表面へめっきする際に用いるストライクめっき液に蓄積する亜鉛を，酸性有機リン抽出剤を用いて選択除去し，ストライクめっき液の寿命を3–5倍に延ばすプロセスを確立した．"}],"abstractLicenseFlag":"disallow"}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1420282801206071552","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"20357437"},{"@type":"NRID","@value":"1000020357437"},{"@type":"NRID","@value":"9000258674909"},{"@type":"NRID","@value":"9000018757955"},{"@type":"NRID","@value":"9000010365566"},{"@type":"NRID","@value":"9000002182208"},{"@type":"NRID","@value":"9000001789850"},{"@type":"NRID","@value":"9000018804736"},{"@type":"NRID","@value":"9000003650842"},{"@type":"NRID","@value":"9000345291306"},{"@type":"NRID","@value":"9000347088774"},{"@type":"NRID","@value":"9000273000527"},{"@type":"NRID","@value":"9000000080886"},{"@type":"NRID","@value":"9000353372195"},{"@type":"NRID","@value":"9000258577988"},{"@type":"NRID","@value":"9000020157561"},{"@type":"NRID","@value":"9000370282506"},{"@type":"NRID","@value":"9000283865388"},{"@type":"NRID","@value":"9000257845670"},{"@type":"NRID","@value":"9000283614739"},{"@type":"NRID","@value":"9000301747446"},{"@type":"NRID","@value":"9000376926044"},{"@type":"NRID","@value":"9000257845825"},{"@type":"NRID","@value":"9000242711444"},{"@type":"NRID","@value":"9000007627015"},{"@type":"NRID","@value":"9000261668399"},{"@type":"NRID","@value":"9000277060689"},{"@type":"NRID","@value":"9000258679895"},{"@type":"NRID","@value":"9000256896573"},{"@type":"NRID","@value":"9000283851263"},{"@type":"NRID","@value":"9000254770394"},{"@type":"NRID","@value":"9000257844650"},{"@type":"NRID","@value":"9000264866415"},{"@type":"NRID","@value":"9000010146340"},{"@type":"NRID","@value":"9000001317747"},{"@type":"NRID","@value":"9000367054084"},{"@type":"NRID","@value":"9000283859495"},{"@type":"NRID","@value":"9000392597995"},{"@type":"NRID","@value":"9000392125029"},{"@type":"NRID","@value":"9000009744107"},{"@type":"NRID","@value":"9000021673088"},{"@type":"NRID","@value":"9000257722531"},{"@type":"NRID","@value":"9000009852254"},{"@type":"NRID","@value":"9000007028105"},{"@type":"NRID","@value":"9000020697483"},{"@type":"NRID","@value":"9000283834848"},{"@type":"NRID","@value":"9000323843210"},{"@type":"NRID","@value":"9000257844696"},{"@type":"NRID","@value":"9000242713987"},{"@type":"NRID","@value":"9000241881738"},{"@type":"NRID","@value":"9000283911943"},{"@type":"NRID","@value":"9000283854120"},{"@type":"NRID","@value":"9000256434877"},{"@type":"NRID","@value":"9000332223801"},{"@type":"NRID","@value":"9000242741935"},{"@type":"NRID","@value":"9000361254544"},{"@type":"NRID","@value":"9000009880840"},{"@type":"NRID","@value":"9000001712544"},{"@type":"NRID","@value":"9000010139259"},{"@type":"NRID","@value":"9000277060687"},{"@type":"NRID","@value":"9000283854880"},{"@type":"NRID","@value":"9000283865384"},{"@type":"NRID","@value":"9000257738150"},{"@type":"NRID","@value":"9000009250765"},{"@type":"NRID","@value":"9000386206393"},{"@type":"NRID","@value":"9000257829117"},{"@type":"NRID","@value":"9000333080396"},{"@type":"NRID","@value":"9000010547837"},{"@type":"NRID","@value":"9000010638995"},{"@type":"NRID","@value":"9000283911826"},{"@type":"NRID","@value":"9000309571594"},{"@type":"NRID","@value":"9000242713972"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/read0004683"}],"foaf:name":[{"@language":"en","@value":"Tanaka Mikiya"},{"@language":"ja","@value":"田中 幹也"}],"jpcoar:affiliationName":[{"@language":"en","@value":"Research Institute for Environmental Management Technology, National Institute of Advanced Industrial Science and Technology (AIST)"},{"@language":"ja","@value":"（独）産業技術総合研究所 環境管理技術研究部門"}]},{"@id":"https://cir.nii.ac.jp/crid/1410001204511125251","@type":"Researcher","personIdentifier":[{"@type":"NRID","@value":"9000010365564"},{"@type":"NRID","@value":"9000353372194"},{"@type":"NRID","@value":"9000001318397"},{"@type":"NRID","@value":"9000370282502"},{"@type":"NRID","@value":"9000376926043"},{"@type":"NRID","@value":"9000256896572"},{"@type":"NRID","@value":"9000001317746"},{"@type":"NRID","@value":"9000367054083"},{"@type":"NRID","@value":"9000412667358"},{"@type":"NRID","@value":"9000257722530"},{"@type":"NRID","@value":"9000323843209"},{"@type":"NRID","@value":"9000009880818"},{"@type":"NRID","@value":"9000361254542"},{"@type":"NRID","@value":"9000009880838"},{"@type":"NRID","@value":"9000257738149"},{"@type":"NRID","@value":"9000283911825"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/hirokazu-narita"}],"foaf:name":[{"@language":"en","@value":"Narita Hirokazu"},{"@language":"ja","@value":"成田 弘一"}],"jpcoar:affiliationName":[{"@language":"en","@value":"Research Institute for Environmental Management Technology, National Institute of Advanced Industrial Science and Technology (AIST)"},{"@language":"ja","@value":"（独）産業技術総合研究所 環境管理技術研究部門"}]},{"@id":"https://cir.nii.ac.jp/crid/1410853646758980736","@type":"Researcher","personIdentifier":[{"@type":"NRID","@value":"9000000326903"}],"foaf:name":[{"@language":"en","@value":"Saiki Yukinori"},{"@language":"ja","@value":"齋木 幸則"}],"jpcoar:affiliationName":[{"@language":"en","@value":"Japan Kanigen Co., Ltd."},{"@language":"ja","@value":"日本カニゼン（株）"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"0386216X"},{"@type":"LISSN","@value":"0386216X"},{"@type":"EISSN","@value":"13499203"},{"@type":"NDL_BIB_ID","@value":"000000026852"},{"@type":"ISSN","@value":"0386216X"},{"@type":"NCID","@value":"AN00037234"}],"prism:publicationName":[{"@language":"en","@value":"KAGAKU KOGAKU RONBUNSHU"},{"@language":"ja","@value":"化学工学論文集"},{"@language":"en","@value":"KAGAKU KOGAKU RONBUNSHU"},{"@language":"ja","@value":"化学工学論文集"}],"dc:publisher":[{"@language":"en","@value":"The Society of Chemical Engineers, Japan"},{"@language":"ja","@value":"公益社団法人 化学工学会"}],"prism:publicationDate":"2010","prism:volume":"36","prism:number":"4","prism:startingPage":"201","prism:endingPage":"206"},"reviewed":"false","url":[{"@id":"http://id.ndl.go.jp/bib/10784734"},{"@id":"https://ndlsearch.ndl.go.jp/books/R000000004-I10784734"},{"@id":"http://www.jstage.jst.go.jp/article/kakoronbunshu/36/4/36_4_201/_pdf"}],"availableAt":"2010","foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=Electroless%20Nickel%20Plating","dc:title":"Electroless Nickel Plating"},{"@id":"https://cir.nii.ac.jp/all?q=Solvent%20Extraction","dc:title":"Solvent Extraction"},{"@id":"https://cir.nii.ac.jp/all?q=Recycling","dc:title":"Recycling"},{"@id":"https://cir.nii.ac.jp/all?q=LIX84I","dc:title":"LIX84I"},{"@id":"https://cir.nii.ac.jp/all?q=PC88A","dc:title":"PC88A"},{"@id":"https://cir.nii.ac.jp/all?q=%E7%84%A1%E9%9B%BB%E8%A7%A3%E3%83%8B%E3%83%83%E3%82%B1%E3%83%AB%E3%82%81%E3%81%A3%E3%81%8D","dc:title":"無電解ニッケルめっき"},{"@id":"https://cir.nii.ac.jp/all?q=%E6%BA%B6%E5%AA%92%E6%8A%BD%E5%87%BA","dc:title":"溶媒抽出"},{"@id":"https://cir.nii.ac.jp/all?q=%E3%83%AA%E3%82%B5%E3%82%A4%E3%82%AF%E3%83%AB","dc:title":"リサイクル"},{"@id":"https://cir.nii.ac.jp/all?q=LIX84I","dc:title":"LIX84I"},{"@id":"https://cir.nii.ac.jp/all?q=PC88A","dc:title":"PC88A"}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1050288789745883392","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Extraction Rate of Nickel with 5-Dodecylsalicylaldoxime in a 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extractor"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204114028416","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"２１世紀を支える表面技術　　無電解ニッケルめっき老化液処理の現況"},{"@language":"en","@value":"A Present Study of Wastewater Treatment for Electroless Nickel Plating"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204118129024","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"ja","@value":"高機能吸着材による資源循環型排水処理"},{"@language":"en","@value":"Metal Resource-Circulating Treatment of Plating Drainage by Using Advanced Adsorbent"},{"@language":"ja-Kana","@value":"コウキノウ キュウチャクザイ ニ ヨル シゲン ジュンカンガタ ハイスイ ショリ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204513409408","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"ja","@value":"高圧力下での無電解ニッケル–リンめっき"},{"@language":"en","@value":"Electroless Nickel–Phosphorus Plating under High Pressure"},{"@language":"ja-Kana","@value":"コウアツリョク カ デ ノ ムデンカイ ニッケル-リンメッキ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204566327040","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Holdup of dispersed phase in a mixer-settler extraction column."}]},{"@id":"https://cir.nii.ac.jp/crid/1390001205208425344","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Analysis of Extraction Rate of Phosphorous Acid with Tri-n-octylamine in Toluene Using a Vibration Type Extractor"},{"@language":"ja","@value":"振動型反応器を用いたトリ－ｎ－オクチルアミンのトルエン溶液による亜リン酸の抽出速度の解析"},{"@language":"ja-Kana","@value":"シンドウガタ ハンノウキ オ モチイタ トリ n オクチルアミン ノ トルエン ヨウエキ ニ ヨル アリンサン ノ チュウシュツ ソクド ノ カイセキ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001205980604544","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"ja","@value":"Acorga P-5100による塩酸溶液からのCu (II) の溶媒抽出平衡"},{"@language":"en","@value":"Solvent Extraction Equilibria of Cu (II) from Hydrochloric Acid Solutions with Acorga P-5100"},{"@value":"Acorga P-5100による塩酸溶液からのCu(2)の溶媒抽出平衡"},{"@language":"ja-Kana","@value":"Acorga P-5100 ニ ヨル エンサン ヨウエキ カラ ノ Cu 2"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001206017155584","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Recovery of Nickel from Spent Electroless Nickel Plating Baths by Solvent Extraction Using LIX84I."},{"@language":"ja","@value":"ＬＩＸ８４Ｉを用いた溶媒抽出法による使用済み無電解ニッケルめっき浴からのニッケルの分離回収"},{"@language":"ja-Kana","@value":"LIX84I オ モチイタ ヨウバイ チュウシュツホウ ニ ヨル シヨウズミ ムデンカイ ニッケルメッキ ヨク カラ ノ ニッケル ノ ブンリ カイシュウ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001206485279232","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@language":"ja","@value":"種々の抽出剤によるアンモニウム塩水溶液からの金属イオンの溶媒抽出"},{"@language":"en","@value":"Extraction of Metal Ions from Ammoniacal Solution with Various Extractants"},{"@language":"ja-Kana","@value":"シュジュ ノ チュウシュツザイ ニ ヨル アンモニウムエン スイヨウエキ カラ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001288142376704","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Preparation of Carbonaceous Sulfur-impregnated Adsorbent from Rice Straw for Nickel Recovery from Nickelplating Waste Solution"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282679094835456","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"ja","@value":"エマルションフロー抽出法による 使用済み無電解ニッケルめっき液からのニッケルリサイクル"},{"@language":"en","@value":"Nickel Recycling from Spent Electroless Nickel Plating Baths Using Emulsion Flow Extractor"},{"@language":"ja-Kana","@value":"エマルションフロー チュウシュツホウ ニ ヨル シヨウ ズミ ムデンカイ ニッケルメッキ エキ カラ ノ ニッケルリサイクル"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282679104974208","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Interfacial phenomena in the extraction kinetics of nickel(II) with 2'-hydroxy-5'-nonylacetophenone oxime."},{"@value":"Interfacial Phenomena in the Extraction Kinetics of Nickel(II) with 2′-Hydroxy-5′-nonylacetophenone Oxime"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282680185135360","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Recovery of Acids Components from Spent Electroless Nickel Plating Bath Using Closed Circulation Type Continuous Extraction Equipment"},{"@language":"ja","@value":"閉鎖循環型連続抽出装置を用いた　無電解ニッケルめっき廃液からの酸成分の分離回収"},{"@language":"ja-Kana","@value":"ヘイサ ジュンカンガタ レンゾク チュウシュツ ソウチ オ モチイタ ムデンカイ ニッケル メッキ ハイエキ カラノ サン セイブン ノ ブンリ カイシュウ"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282680717860224","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Continuous Liquid-Liquid Extraction of Nickel from Simulated Electroless Nickel Plating Liquid Wastes by Using a Counter Current Emulsion Flow Extractor"},{"@value":"Continuous Liquid-Liquid 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