{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1390282679527216384.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.2343/geochemj.1.0018"}},{"identifier":{"@type":"COI","@value":"1:CAS:528:DC%2BD1MXhtVeltL%2FP"}},{"identifier":{"@type":"NDL_BIB_ID","@value":"10264049"}},{"identifier":{"@type":"URI","@value":"http://id.ndl.go.jp/bib/10264049"}},{"identifier":{"@type":"URI","@value":"https://ndlsearch.ndl.go.jp/books/R000000004-I10264049"}},{"identifier":{"@type":"URI","@value":"http://www.jstage.jst.go.jp/article/geochemj/43/3/43_1.0018/_pdf"}},{"identifier":{"@type":"NAID","@value":"130004469255"}},{"identifier":{"@type":"NAID","@value":"10026141523"}}],"dc:title":[{"@language":"en","@value":"Comprehensive analysis for major, minor and trace element contents and Sr-Nd-Pb-Hf isotope ratios in sediment reference materials, JSd-1 and MAG-1"}],"dc:language":"en","description":[{"type":"abstract","notation":[{"@language":"en","@value":"In view of the requirement of a well-characterized and easily available aquatic sediment reference material, a comprehensive analysis comprising of fifty major, minor and trace elements as well as Sr-Nd-Pb-Hf isotopes were carried out in the stream sediment reference material, JSd-1, issued by the Geological Survey of Japan. The data for marine sediment reference material, MAG-1, issued by U.S. Geological Survey is also obtained for comparison. The elements were divided into two groups: Group I and Group II. Elements in Group I form stable soluble ions in HNO<sub>3</sub>; and those in Group II form soluble oxo- and fluoro-complexes in HF, such as Zr, Nb, Hf, Ta, etc. For Group I, the sample was decomposed with HF in a tetra fluoro ethylene (TFE) bomb at 245°C for 96 hrs with Mg addition. The elemental concentration was measured by quadrupole type inductively coupled plasma source mass spectrometry (ICP-QMS) and sector field type ICP-MS (ICP-SFMS) using isotope dilution-internal standardization (ID-IS) methods. The aliquot of the sample solution was passed through 3-step column chemistry for isotope ratio determination of Pb by multiple collector (MC) ICP-MS and thermal ionization mass spectrometry (TIMS), and Sr and Nd by TIMS. For Group II elements, the sample was decomposed with HF in a TFE bomb with the same time and temperature settings. Zr, Mo, Sn, Sb and Hf were determined by ID, and Nb and Ta by ID-IS using ICP-QMS. The original JSd-1 powder showed heterogeneity for Group II elements, indicating insufficient pulverization and distribution. Thus, we further pulverized the powder and measured the concentration, which showed improved homogeneity. The aliquot for the re-pulverized powder was passed through 2-step column chemistry, and the Hf isotope ratio was determined by MC-ICP-MS. Thus a new data on the trace elements as well as Sr-Nd-Pb-Hf isotope ratios is provided for JSd-1 and MAG-1 in this paper."}],"abstractLicenseFlag":"disallow"}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1410282679527216385","@type":"Researcher","personIdentifier":[{"@type":"NRID","@value":"9000257916950"}],"foaf:name":[{"@language":"en","@value":"NAGENDER NATH B."}],"jpcoar:affiliationName":[{"@language":"en","@value":"The Pheasant Memorial Laboratory for Geochemistry and Cosmochemistry (PML), Institute for Study of the Earth's Interior, Okayama University"},{"@language":"en","@value":"National Institute of Oceanography"}]},{"@id":"https://cir.nii.ac.jp/crid/1420564276188038144","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"70219301"},{"@type":"NRID","@value":"1000070219301"},{"@type":"NRID","@value":"9000020554678"},{"@type":"NRID","@value":"9000254146412"},{"@type":"NRID","@value":"9000021766200"},{"@type":"NRID","@value":"9000020656375"},{"@type":"NRID","@value":"9000257794804"},{"@type":"NRID","@value":"9000020758245"},{"@type":"NRID","@value":"9000018329361"},{"@type":"NRID","@value":"9000254111567"},{"@type":"NRID","@value":"9000021096209"},{"@type":"NRID","@value":"9000253675205"},{"@type":"NRID","@value":"9000257916951"},{"@type":"NRID","@value":"9000283783366"},{"@type":"NRID","@value":"9000254530248"},{"@type":"NRID","@value":"9000254530176"},{"@type":"NRID","@value":"9000258005004"},{"@type":"NRID","@value":"9000258406506"},{"@type":"NRID","@value":"9000002108690"},{"@type":"NRID","@value":"9000257916840"},{"@type":"NRID","@value":"9000283906883"},{"@type":"NRID","@value":"9000258435068"},{"@type":"NRID","@value":"9000020236299"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/AkioMakishima"}],"foaf:name":[{"@language":"en","@value":"MAKISHIMA AKIO"}],"jpcoar:affiliationName":[{"@language":"en","@value":"The Pheasant Memorial Laboratory for Geochemistry and Cosmochemistry (PML), Institute for Study of the Earth's Interior, Okayama University"}]},{"@id":"https://cir.nii.ac.jp/crid/1410282679527216387","@type":"Researcher","personIdentifier":[{"@type":"NRID","@value":"9000257916952"},{"@type":"NRID","@value":"9000017180358"}],"foaf:name":[{"@language":"en","@value":"NOORDMANN JANINE"}],"jpcoar:affiliationName":[{"@language":"en","@value":"The Pheasant Memorial Laboratory for Geochemistry and Cosmochemistry (PML), Institute for Study of the Earth's Interior, Okayama 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RYOJI"}],"jpcoar:affiliationName":[{"@language":"en","@value":"The Pheasant Memorial Laboratory for Geochemistry and Cosmochemistry (PML), Institute for Study of the Earth's Interior, Okayama University"}]},{"@id":"https://cir.nii.ac.jp/crid/1030003658401333889","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"80201672"},{"@type":"NRID","@value":"1000080201672"},{"@type":"NRID","@value":"9000258435178"},{"@type":"NRID","@value":"9000391814813"},{"@type":"NRID","@value":"9000408871240"},{"@type":"NRID","@value":"9000283783520"},{"@type":"NRID","@value":"9000408782704"},{"@type":"NRID","@value":"9000018329360"},{"@type":"NRID","@value":"9000021096203"},{"@type":"NRID","@value":"9000283783497"},{"@type":"NRID","@value":"9000345324031"},{"@type":"NRID","@value":"9000020170930"},{"@type":"NRID","@value":"9000020434270"},{"@type":"NRID","@value":"9000020571523"},{"@type":"NRID","@value":"9000391814862"},{"@type":"NRID","@value":"9000391814682"},{"@type":"NRID","@value":"9000000519294"},{"@type":"NRID","@value":"9000020055008"},{"@type":"NRID","@value":"9000391848816"},{"@type":"NRID","@value":"9000006894532"},{"@type":"NRID","@value":"9000004619598"},{"@type":"NRID","@value":"9000254146469"},{"@type":"NRID","@value":"9000391814817"},{"@type":"NRID","@value":"9000257916954"},{"@type":"NRID","@value":"9000020759332"},{"@type":"NRID","@value":"9000283783367"},{"@type":"NRID","@value":"9000020090865"},{"@type":"NRID","@value":"9000391814975"},{"@type":"NRID","@value":"9000254589436"},{"@type":"NRID","@value":"9000002108692"},{"@type":"NRID","@value":"9000254150846"},{"@type":"NRID","@value":"9000402605739"},{"@type":"NRID","@value":"9000370745960"},{"@type":"NRID","@value":"9000391814965"},{"@type":"NRID","@value":"9000257916842"},{"@type":"NRID","@value":"9000391989006"},{"@type":"NRID","@value":"9000020236305"},{"@type":"NRID","@value":"9000283783379"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/read0016189"}],"foaf:name":[{"@language":"en","@value":"NAKAMURA EIZO"}],"jpcoar:affiliationName":[{"@language":"en","@value":"The Pheasant Memorial Laboratory for Geochemistry and Cosmochemistry (PML), Institute for Study of the Earth's Interior, Okayama University"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"00167002"},{"@type":"LISSN","@value":"00167002"},{"@type":"EISSN","@value":"18805973"},{"@type":"NDL_BIB_ID","@value":"000000128646"},{"@type":"ISSN","@value":"00167002"},{"@type":"NCID","@value":"AA00654975"}],"prism:publicationName":[{"@language":"en","@value":"GEOCHEMICAL JOURNAL"},{"@language":"ja","@value":"ＧＥＯＣＨＥＭＩＣＡＬ　ＪＯＵＲＮＡＬ"},{"@language":"en","@value":"Geochem. J."},{"@language":"ja","@value":"Ｇｅｏｃｈｅｍ．　Ｊ．"}],"dc:publisher":[{"@language":"en","@value":"GEOCHEMICAL SOCIETY OF JAPAN"},{"@language":"ja","@value":"一般社団法人日本地球化学会"}],"prism:publicationDate":"2009","prism:volume":"43","prism:number":"3","prism:startingPage":"207","prism:endingPage":"216"},"reviewed":"false","dcterms:accessRights":"http://purl.org/coar/access_right/c_abf2","url":[{"@id":"http://id.ndl.go.jp/bib/10264049"},{"@id":"https://ndlsearch.ndl.go.jp/books/R000000004-I10264049"},{"@id":"http://www.jstage.jst.go.jp/article/geochemj/43/3/43_1.0018/_pdf"}],"availableAt":"2009","foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=sediment%20standard","dc:title":"sediment standard"},{"@id":"https://cir.nii.ac.jp/all?q=JSd-1","dc:title":"JSd-1"},{"@id":"https://cir.nii.ac.jp/all?q=MAG-1","dc:title":"MAG-1"},{"@id":"https://cir.nii.ac.jp/all?q=trace%20elements","dc:title":"trace elements"},{"@id":"https://cir.nii.ac.jp/all?q=Sr-Nd-Pb-Hf%20isotope%20ratios","dc:title":"Sr-Nd-Pb-Hf isotope ratios"}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1360011145160558080","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Coprecipitation of Ti, Mo, Sn and Sb with fluorides and application to determination of B, Ti, Zr, Nb, Mo, Sn, Sb, Hf and Ta by ICP-MS"}]},{"@id":"https://cir.nii.ac.jp/crid/1360011146279816960","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@value":"Evaluation of the coprecipitation of incompatible trace elements with fluoride during silicate rock dissolution by acid digestion"}]},{"@id":"https://cir.nii.ac.jp/crid/1360574094250431360","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Precise determination of Pb isotope ratios by simple double spike MC-ICP-MS technique without Tl addition"}]},{"@id":"https://cir.nii.ac.jp/crid/1360855568905181312","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Determination of Major/ Minor and Trace Elements in Silicate Samples by ICP‐QMS and ICP‐SFMS Applying Isotope Dilution‐Internal Standardisation (ID‐IS) and Multi‐Stage Internal Standardisation"}]},{"@id":"https://cir.nii.ac.jp/crid/1360855570312314624","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Trace and rare earth elemental variation in Arabian Sea sediments through a transect across the oxygen minimum zone"}]},{"@id":"https://cir.nii.ac.jp/crid/1361137045118512256","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@value":"The composition of the Earth"}]},{"@id":"https://cir.nii.ac.jp/crid/1361699994294071040","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"1994 COMPILATION OF WORKING VALUES AND SAMPLE DESCRIPTION FOR 383 GEOSTANDARDS"}]},{"@id":"https://cir.nii.ac.jp/crid/1362544420920126976","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"1998 Compilation of Analytical Data for Five GSJ Geochemical Reference Samples: The “Instrumental Analysis Series”"}]},{"@id":"https://cir.nii.ac.jp/crid/1362825896319830016","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Preparation of Two New GSJ Geochemical Reference Materials: Basalt JB‐1b and Coal Fly Ash JCFA‐1"}]},{"@id":"https://cir.nii.ac.jp/crid/1363107371081354752","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Purification of Hf in silicate materials using extraction chromatographic resin, and its application to precise determination of<sup>176</sup>Hf/<sup>177</sup>Hf by MC-ICP-MS with<sup>179</sup>Hf spike"}]},{"@id":"https://cir.nii.ac.jp/crid/1363388845284892160","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Precise isotope analysis of nanogram-level Pb for natural rock samples without use of double spikes"}]},{"@id":"https://cir.nii.ac.jp/crid/1363388846354441088","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Suppression of Matrix Effects in ICP‐MS by High Power Operation of ICP: Application to Precise Determination of Rb, Sr, Y, Cs, Ba, REE, Pb, Th and U at ng g<sup>‐1</sup> Levels in Milligram Silicate Samples"}]},{"@id":"https://cir.nii.ac.jp/crid/1363951794996834944","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Influence of Provenance, Weathering, and Sedimentary Processes on the Elemental Ratios of the Fine-Grained Fraction of the Bedload Sediments from the Vembanad Lake and the Adjoining Continental Shelf, Southwest Coast of India"}]},{"@id":"https://cir.nii.ac.jp/crid/1364233269088681344","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Highly precise and accurate isotopic analysis of small amounts of Pb using<sup>205</sup>Pb–<sup>204</sup>Pb and<sup>207</sup>Pb-<sup>204</sup>Pb, two double spikes"}]},{"@id":"https://cir.nii.ac.jp/crid/1364233270231035776","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"1996 COMPILATION OF ANALYTICAL DATA ON NINE GSJ GEOCHEMICAL REFERENCE SAMPLES, “SEDIMENTARY ROCK SERIES”"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204144763264","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Formation and suppression of AlF<sub>3</sub> during HF digestion of rock samples in Teflon bomb for precise trace element analyses by ICP-MS and ID-TIMS"},{"@value":"Formation and suppression of AlF3 during HF digestion of rock samples in Teflon bomb for precise trace element analyses by ICP-MS and ID-TIMS"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204550016128","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Precise determination of REE for sedimentary reference rocks issued by the Geological Survey of Japan"}]},{"@id":"https://cir.nii.ac.jp/crid/1390001204550419456","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"1994 compilation values for GSJ reference samples, \"Igneous rock series\"."},{"@value":"1994 compilation values for CSJ reference samples, “Igneous rock series”"},{"@value":"1994 compilation values for GSJ reference samples, “Igneous rock series” (letter)"},{"@value":"compilation values for GSJ reference samples, igneous rock series"},{"@value":"1994 compilation of analytical data for minor and trace elements in seventeen GSJ geochemical reference samples, “igneous rock series”"},{"@value":"994 compilation values for GSJ reference samples, “Igneous rock series”"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282679233848704","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Lead Isotopic Compositions of Environmental Certified Reference Materials for an Inter-Laboratory Comparison of Lead Isotope Analysis"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282679234375424","@type":"Article","relationType":["isReferencedBy","isCitedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Precise Elemental and Isotopic Analyses in Silicate Samples Employing ICP-MS: Application of Hydrofluoric Acid Solution and Analytical Techniques"}]},{"@id":"https://cir.nii.ac.jp/crid/1390282679527516672","@type":"Article","relationType":["references","cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"New sequential separation procedure for Sr, Nd and Pb isotope ratio measurement in geological material using MC-ICP-MS and TIMS"}]},{"@id":"https://cir.nii.ac.jp/crid/1390298146220360832","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Single column REE separation and radiogenic <sup>143</sup>Nd/<sup>144</sup>Nd analysis without Sm elimination"}]},{"@id":"https://cir.nii.ac.jp/crid/1390858608267618816","@type":"Article","relationType":["isReferencedBy"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Sequential Pb-Sr-LREE separation from silicates for isotopic analysis"}]},{"@id":"https://cir.nii.ac.jp/crid/1570291226069448192","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Preparation of two new GSJ geochemical reference materials : JB-1b and coal fly ash JCFA-1"}]},{"@id":"https://cir.nii.ac.jp/crid/1571135650037087616","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Influence of Provenance, weathering, and sedimentary processes on the elemental ratios of the fine-grained fraction of the bedload sediments from the Vembanad Lake and the adjoining continental shelf, southwest coast of India"}]},{"@id":"https://cir.nii.ac.jp/crid/1571980075929711488","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Geochemistry of sediments"}]},{"@id":"https://cir.nii.ac.jp/crid/1571980075929715328","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Determination of major, minor and trace elements in silicate samples by ICP-QMS and ICP-SFMS applying isotope dilution-internal standardization (ID-IS) and multi-stage internal standardisation"}]},{"@id":"https://cir.nii.ac.jp/crid/1571980076666605568","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Highly precise and accurate isotopic analysis of small amounts of Pb using ^<205>Pb-^<204>Pb and ^<207>Pb-^<204>Pb, two double spikes"}]},{"@id":"https://cir.nii.ac.jp/crid/1572261551376140160","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Precise determination of Pb isotope ratios by simple double spike MC-ICP-MS technique without Tl addition"}]},{"@id":"https://cir.nii.ac.jp/crid/1572543025690480512","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Trace and rare-earth elemental variations in Arabian Sea sediments through a transect across the oxygen minimum zone"}]},{"@id":"https://cir.nii.ac.jp/crid/1573387450813263744","@type":"Article","relationType":["cites"]},{"@id":"https://cir.nii.ac.jp/crid/1573387451283029888","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Purification of Hf in silicate materials using extraction chromatographic resin, and its application to precise determination of ^<176>Hf/ ^<177>Hf by MC-ICP-MS with ^<179>Hf spike"}]},{"@id":"https://cir.nii.ac.jp/crid/1573387451849488640","@type":"Article","resourceType":"学術雑誌論文(journal article)","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Comprehensive geochemical analyses of small amounts (<100 mg) of extraterrestrial samples for the analytical competition related to the sample return mission MUSES-C"},{"@value":"Comprehensive geochemical analyses of small amounts (100 mg) of extraterrestrial samples for the analytical competition related to the sample‐return mission, MUSES‐C"}]},{"@id":"https://cir.nii.ac.jp/crid/1573668925789975552","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Suppression of matrix effects in ICP-MS by high power operation of ICP : Application to precise determination of Rb, Sr, Y, Cs, Ba, REE, Pb, Th and U at ng g^<-1> levels in milligram silicate samples"}]},{"@id":"https://cir.nii.ac.jp/crid/1573668926258321920","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Coprecipitation of Ti, Mo, Sn and Sb with fluorides and application to determination of B, Ti, Zr, Nb, Mo, Sn, Sb, Hf and Ta by ICP-MS"}]},{"@id":"https://cir.nii.ac.jp/crid/1573950400766686464","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"1998 compilation of analytical data for five GSJ geochemical reference samples : The \"Instrumental Analysis Series\""}]},{"@id":"https://cir.nii.ac.jp/crid/1574231875743395840","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"1996 compilation of analytical data on nine GSJ geochemical reference samples, \"Sedimentary rock series\""}]},{"@id":"https://cir.nii.ac.jp/crid/1574231876472606720","@type":"Article","relationType":["cites"],"jpcoar:relatedTitle":[{"@language":"en","@value":"Precise isotope 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