{"@context":{"@vocab":"https://cir.nii.ac.jp/schema/1.0/","rdfs":"http://www.w3.org/2000/01/rdf-schema#","dc":"http://purl.org/dc/elements/1.1/","dcterms":"http://purl.org/dc/terms/","foaf":"http://xmlns.com/foaf/0.1/","prism":"http://prismstandard.org/namespaces/basic/2.0/","cinii":"http://ci.nii.ac.jp/ns/1.0/","datacite":"https://schema.datacite.org/meta/kernel-4/","ndl":"http://ndl.go.jp/dcndl/terms/","jpcoar":"https://github.com/JPCOAR/schema/blob/master/2.0/"},"@id":"https://cir.nii.ac.jp/crid/1390282681264944640.json","@type":"Article","productIdentifier":[{"identifier":{"@type":"DOI","@value":"10.1295/polymj.34.593"}},{"identifier":{"@type":"COI","@value":"1:CAS:528:DC%2BD38XmvFWjsLg%3D"}},{"identifier":{"@type":"NDL_BIB_ID","@value":"6285432"}},{"identifier":{"@type":"URI","@value":"http://id.ndl.go.jp/bib/6285432"}},{"identifier":{"@type":"URI","@value":"https://ndlsearch.ndl.go.jp/books/R000000004-I6285432"}},{"identifier":{"@type":"NAID","@value":"10012289631"}}],"dc:title":[{"@language":"en","@value":"Crystallization Process in Binary Blends of Poly(.EPSILON.-caprolactone)-block-Polybutadiene Copolymers."},{"@value":"Crystallization Process in Binary Blends of Poly(ε-caprolactone)-block-Polybutadiene Copolymers"},{"@language":"ja-Kana","@value":"Crystallization Process in Binary Blends of Poly イプシロン caprolactone block Polybutadiene Copolymers"}],"dc:language":"en","description":[{"type":"abstract","notation":[{"@language":"en","@value":"The crystallization process in binary blends of poly(ε-caprolactone)-<I>block</I>-polybutadiene (PCL-<I>b</I>-PB) copolymers has been investigated by time-resolved small-angle X-Ray scattering with synchrotron radiation (SR-SAXS), where the crystallization of PCL blocks induces a morphological transition both in neat copolymers but the crystallization rate is extremely different between them. The microdomain structure in the melt and the final morphology after crystallization were also measured by conventional SAXS, and the melting behavior of crystallized samples was observed by differential scanning calorimetry (DSC). The binary blend forms a single microdomain structure in the melt over the whole composition range investigated, and the crystallization proceeds with an intermediate rate between those of the constituent PCL-<I>b</I>-PB copolymers to result in a single lamellar morphology. The time dependence of SR-SAXS curves is qualitatively similar in features to that for the crystallization of pure PCL-<I>b</I>-PB copolymers, suggesting that the crystallization of the blend is substantially controlled by a single crystallization mechanism. The remarkable change in the crystallization rate with composition is ascribed to the difference in the stability of preexisting microdomain structures. The conformation of (longer and shorter) PB blocks in the final lamellar morphology is qualitatively discussed."}],"abstractLicenseFlag":"disallow"}],"creator":[{"@id":"https://cir.nii.ac.jp/crid/1410282681264944640","@type":"Researcher","personIdentifier":[{"@type":"NRID","@value":"9000001151814"}],"foaf:name":[{"@language":"en","@value":"Ito Kazuhiro"}],"jpcoar:affiliationName":[{"@language":"en","@value":"School of Materials Science, Japan Advanced Institute of Science and Technology (JAIST)"}]},{"@id":"https://cir.nii.ac.jp/crid/1410282681264944644","@type":"Researcher","foaf:name":[{"@language":"en","@value":"Tanimoto Satoshi"}],"jpcoar:affiliationName":[{"@language":"en","@value":"School of Materials Science, Japan Advanced Institute of Science and Technology (JAIST)"}]},{"@id":"https://cir.nii.ac.jp/crid/1410001205227554821","@type":"Researcher","personIdentifier":[{"@type":"NRID","@value":"9000000191933"},{"@type":"NRID","@value":"9000016379052"},{"@type":"NRID","@value":"9000257860300"},{"@type":"NRID","@value":"9000254934740"},{"@type":"NRID","@value":"9000283596225"},{"@type":"NRID","@value":"9000283596232"},{"@type":"NRID","@value":"9000001151819"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/read0098628"}],"foaf:name":[{"@language":"en","@value":"Takeshita Hiroki"}],"jpcoar:affiliationName":[{"@language":"en","@value":"Department of Material Science and Technology, Nagaoka University of Technology"}]},{"@id":"https://cir.nii.ac.jp/crid/1410282681264944643","@type":"Researcher","foaf:name":[{"@language":"en","@value":"Sasaki Shintaro"}],"jpcoar:affiliationName":[{"@language":"en","@value":"School of Materials Science, Japan Advanced Institute of Science and Technology (JAIST)"}]},{"@id":"https://cir.nii.ac.jp/crid/1030003658364585856","@type":"Researcher","personIdentifier":[{"@type":"KAKEN_RESEARCHERS","@value":"20156194"},{"@type":"NRID","@value":"1000020156194"},{"@type":"NRID","@value":"9000257747607"},{"@type":"NRID","@value":"9000256200786"},{"@type":"NRID","@value":"9000020149245"},{"@type":"NRID","@value":"9000257751157"},{"@type":"NRID","@value":"9000002112812"},{"@type":"NRID","@value":"9000283198133"},{"@type":"NRID","@value":"9000014202000"},{"@type":"NRID","@value":"9000403952589"},{"@type":"NRID","@value":"9000014202011"},{"@type":"NRID","@value":"9000021287055"},{"@type":"NRID","@value":"9000257752847"},{"@type":"NRID","@value":"9000257750208"},{"@type":"NRID","@value":"9000265538799"},{"@type":"NRID","@value":"9000257744879"},{"@type":"NRID","@value":"9000257745708"},{"@type":"NRID","@value":"9000017379003"},{"@type":"NRID","@value":"9000283869190"},{"@type":"NRID","@value":"9000020346293"},{"@type":"NRID","@value":"9000283198995"},{"@type":"NRID","@value":"9000283197633"},{"@type":"NRID","@value":"9000283198741"},{"@type":"NRID","@value":"9000256199383"},{"@type":"NRID","@value":"9000283197629"},{"@type":"RESEARCHMAP","@value":"https://researchmap.jp/read0043742"}],"foaf:name":[{"@language":"en","@value":"Nojima Shuichi"}],"jpcoar:affiliationName":[{"@language":"en","@value":"Department of Polymer Chemistry, Tokyo Institute of Technology"}]}],"publication":{"publicationIdentifier":[{"@type":"PISSN","@value":"00323896"},{"@type":"EISSN","@value":"13490540"},{"@type":"NDL_BIB_ID","@value":"000000128645"},{"@type":"ISSN","@value":"00323896"},{"@type":"LISSN","@value":"00323896"},{"@type":"NCID","@value":"AA00777013"}],"prism:publicationName":[{"@language":"en","@value":"Polymer Journal"},{"@language":"en","@value":"Polym. J."}],"dc:publisher":[{"@language":"en","@value":"The Society of Polymer Science, Japan"}],"prism:publicationDate":"2002","prism:volume":"34","prism:number":"8","prism:startingPage":"593","prism:endingPage":"600"},"reviewed":"false","dcterms:accessRights":"http://purl.org/coar/access_right/c_abf2","url":[{"@id":"http://id.ndl.go.jp/bib/6285432"},{"@id":"https://ndlsearch.ndl.go.jp/books/R000000004-I6285432"}],"availableAt":"2002","foaf:topic":[{"@id":"https://cir.nii.ac.jp/all?q=Crystalline-Amorphous%20Diblock%20Copolymer","dc:title":"Crystalline-Amorphous Diblock Copolymer"},{"@id":"https://cir.nii.ac.jp/all?q=Binary%20Blend","dc:title":"Binary Blend"},{"@id":"https://cir.nii.ac.jp/all?q=Crystallization%20Process","dc:title":"Crystallization Process"},{"@id":"https://cir.nii.ac.jp/all?q=Final%20Morphology","dc:title":"Final Morphology"}],"relatedProduct":[{"@id":"https://cir.nii.ac.jp/crid/1360011144407893760","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Chain folding in ethylene-butylene-ethylethylene semicrystalline diblock copolymers"}]},{"@id":"https://cir.nii.ac.jp/crid/1360011144893529472","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Anomalous Temperature Behavior of Lamellar Microdomain Structures in Binary Blends of Polystyrene-<i>block</i>-polyisoprene Diblock Copolymers"}]},{"@id":"https://cir.nii.ac.jp/crid/1360011145305284480","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Crystallization of ε-caprolactone blocks within a crosslinked microdomain structure of poly(ε-caprolactone)-block-polybutadiene"}]},{"@id":"https://cir.nii.ac.jp/crid/1360011146565716224","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Synchrotron SAXS Study of Crystallization and Microphase Separation in Compatible Mixtures of Tetrahydrofuran−Methyl Methacrylate Diblock Copolymer and Poly(tetrahydrofuran)"}]},{"@id":"https://cir.nii.ac.jp/crid/1360292618749439872","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Polymer Crystallization in 25-nm Spheres"}]},{"@id":"https://cir.nii.ac.jp/crid/1360292621480582016","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Crystallization Kinetics of Poly(ethylene oxide) in Poly(ethylene oxide)−Polystyrene−Poly(ethylene oxide) Triblock Copolymers"}]},{"@id":"https://cir.nii.ac.jp/crid/1360574094171334400","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Structural Evolution of Multilayered, Crystalline−Amorphous Diblock Copolymer Thin Films"}]},{"@id":"https://cir.nii.ac.jp/crid/1360855569776064128","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Effect of molecular weight on spherulite growth rates of high molecular weight poly(ethylene oxide) fractions"}]},{"@id":"https://cir.nii.ac.jp/crid/1360855571094531456","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Time-resolved SAXS study of morphological change in a binary blend of poly(iε-caprolactone) and polystyrene oligomer"}]},{"@id":"https://cir.nii.ac.jp/crid/1360855571368985472","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Isothermal Crystallization of Poly(ε-caprolactone−ethylene glycol) Block Copolymers"}]},{"@id":"https://cir.nii.ac.jp/crid/1361137045138872320","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Chain Folding in Semicrystalline Oxyethylene/Oxybutylene Diblock Copolymers"}]},{"@id":"https://cir.nii.ac.jp/crid/1361137045742096128","@type":"Article","relationType":["references"],"jpcoar:relatedTitle":[{"@value":"Time-resolved X-ray study of poly(aryl ether ether ketone) crystallization and melting behaviour: 1. 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