Unusual Selective Monitoring of <i>N,N</i>-Dimethylformamide in a Two-Dimensional Material Field-Effect Transistor

  • Akito Fukui
    Department of Physics and Electronics, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Keigo Matsuyama
    Department of Physics and Electronics, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Hiroaki Onoe
    Department of Mechanical Engineering, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522, Japan
  • Shun Itai
    Department of Mechanical Engineering, Faculty of Science and Technology, Keio University, 3-14-1 Hiyoshi, Kohoku-ku, Yokohama 223-8522, Japan
  • Hidekazu Ikeno
    Department of Materials Science, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Shunsuke Hiraoka
    Department of Materials Science, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Kousei Hiura
    Department of Materials Science, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Yuh Hijikata
    Institute for Chemical Reaction Design and Discovery (WPI-ICReDD), Hokkaido University, Sapporo 001-0021, Japan
  • Jenny Pirillo
    Institute for Chemical Reaction Design and Discovery (WPI-ICReDD), Hokkaido University, Sapporo 001-0021, Japan
  • Takahiro Nagata
    Research Center for Functional Materials, National Institute for Materials Science (NIMS), 1-1 Namiki, Tsukuba 305-0044, Japan
  • Kuniharu Takei
    Department of Physics and Electronics, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Takeshi Yoshimura
    Department of Physics and Electronics, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Norifumi Fujimura
    Department of Physics and Electronics, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan
  • Daisuke Kiriya
    Department of Physics and Electronics, Osaka Metropolitan University, Sakai, Osaka 599-8531, Japan

説明

<jats:p>N,N-Dimethylformamide (DMF) is an essential solvent in industries and pharmaceutics. Its market size range was estimated to be 2 billion US dollars in 2022. Monitoring DMF in solution environments in real time is significant because of its toxicity. However, DMF is not a redox-active molecule; therefore, selective monitoring DMF in solutions in real time requires an unprecedented design at the scale of atomic resolution. In this paper, we propose a selective DMF sensor using a molybdenum disulfide (MoS2) field-effect transistor (FET). The sensor responds to DMF molecules, but not to similar molecules of formamide, N,N-diethylformamide, and N,N-dimethylacetamide. The plausible atomic mechanism is the oxygen substitution sites on MoS2, on which the DMF molecule shows exceptional orientation. The thin structure of MoS2-FET can be incorporated into a microfluidic chamber, which leads to DMF monitoring in real time by exchanging solutions subsequently. The designed device shows DMF monitoring in NaCl ionic solutions from 1 to 200 L/mL. This work proposes the concept of selectively monitoring redox-inactive molecules based on the non-ideal atomic affinity site on the surface of two-dimensional semiconductors.</jats:p>

収録刊行物

  • ACS Nano

    ACS Nano 17 (15), 14981-14989, 2023-07-17

    American Chemical Society (ACS)

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