Synthesis and Isolation of Regiospecific Mono Iodo-Cyclodextrin as a Fragile Intermediate to Amino-Cyclodextrin

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lodo-CD (II) was prepared from toluenesulfonyl-CD (I) and purified by preparative HPLC. Iodo-CD (II) was easily converted to the amino-CD (III). Examination of the structure of the hydrolyzate from amino-CD (III) showed that indination and amination proceeded with inversion of configuration in both reactions.

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KJ00002353278

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