Ion-Based Materials Derived from Positively and Negatively Charged Chloride Complexes of π-Conjugated Molecules

  • Bin Dong
    College of Pharmaceutical Sciences, Ritsumeikan University, Kusatsu 525-8577, Japan
  • Tsuneaki Sakurai
    Department of Applied Chemistry, Graduate School of Engineering, Osaka University, Suita 565-0871, Japan
  • Yuya Bando
    College of Pharmaceutical Sciences, Ritsumeikan University, Kusatsu 525-8577, Japan
  • Shu Seki
    Department of Applied Chemistry, Graduate School of Engineering, Osaka University, Suita 565-0871, Japan
  • Kazuto Takaishi
    Advanced Elements Chemistry Research Team and Elements Chemistry Laboratory, RIKEN, Wako 351-0198, Japan
  • Masanobu Uchiyama
    Advanced Elements Chemistry Research Team and Elements Chemistry Laboratory, RIKEN, Wako 351-0198, Japan
  • Atsuya Muranaka
    Advanced Elements Chemistry Research Team and Elements Chemistry Laboratory, RIKEN, Wako 351-0198, Japan
  • Hiromitsu Maeda
    College of Pharmaceutical Sciences, Ritsumeikan University, Kusatsu 525-8577, Japan

書誌事項

公開日
2013-09-20
資源種別
journal article
DOI
  • 10.1021/ja4071333
公開者
American Chemical Society (ACS)

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説明

Oriented salts from planar charged species were prepared by combining positively and negatively charged receptor-anion complexes with similar geometries using dicationic and electronically neutral π-conjugated receptors. Phenylene- or pyrimidine-bridged bis(imidazolium) dicationic anion receptors formed monocationic receptor-Cl(-) complexes that were accompanied by a free Cl(-). This free Cl(-) was subsequently captured by pyrrole-based neutral anion receptors to form negatively charged receptor-Cl(-) complexes. The ion pair of the resulting positively and negatively charged planar receptor-Cl(-) complexes could produce a supramolecular octane gel, adopting a lamellar self-organized structure in its xerogel state. On the other hand, the solid-state ion pairs had hexagonal columnar mesophases, which formed via alternate stacking of the positively and negatively charged planar receptor-Cl(-) complexes. By use of the flash-photolysis time-resolved microwave conductivity technique, the one-dimensional charge-carrier transporting property, with a mobility of 0.05 cm(2) V(-1) s(-1), was determined for the newly prepared solid-state ion pairs.

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