Stereoselective total synthesis of garsubellin A

書誌事項

公開日
2013-02-06
資源種別
journal article
権利情報
  • http://www.springer.com/tdm
DOI
  • 10.1038/ja.2012.125
公開者
Springer Science and Business Media LLC

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説明

The stereoselective total synthesis of garsubellin A is described. The total synthesis was achieved through the stereoselective construction of a bicyclo[3.3.1]nonane derivative via a three-step sequence: intramolecular cyclopropanation, formation of a germinal dimethyl group, and regioselective ring opening of cyclopropane. To complete the total synthesis of garsubellin A, chemo- and stereoselective hydrogenation to generate the C8 stereogenic center is followed by the formation of the fused tetrahydrofuran ring by a regioselective epoxide-opening reaction with C3 ketone, and finally cross metathesis to construct two prenyl groups.

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