A novel thiochromone-type photolabile protecting group for carbonyl compounds

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説明

A novel photolabile protecting group, thiochromone S,S-dioxide, possessing the 1,2-diol group for protection of ketones and aldehydes is described. Photodeprotection of the successfully protected carbonyl derivatives proceeded smoothly under photoirradiation filtered through Pyrex glass (>280 nm) using an ultrahigh-pressure mercury lamp to recover the corresponding carbonyl compounds and the starting protecting group.

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  • Tetrahedron

    Tetrahedron 69 (19), 3984-3990, 2013-05

    Elsevier BV

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