A single-solenoid pulsed-magnet system for single-crystal scattering studies
-
- Zahirul Islam
- Argonne National Laboratory 1 X-Ray Science Division, Advanced Photon Source, , 9700 S. Cass Ave., Argonne, Illinois 60439, USA
-
- Dana Capatina
- Argonne National Laboratory 2 APS Engineering Support Division, Advanced Photon Source, , 9700 S. Cass Ave., Argonne, Illinois 60439, USA
-
- Jacob P. C. Ruff
- Argonne National Laboratory 1 X-Ray Science Division, Advanced Photon Source, , 9700 S. Cass Ave., Argonne, Illinois 60439, USA
-
- Ritesh K. Das
- Argonne National Laboratory 1 X-Ray Science Division, Advanced Photon Source, , 9700 S. Cass Ave., Argonne, Illinois 60439, USA
-
- Emil Trakhtenberg
- Argonne National Laboratory 2 APS Engineering Support Division, Advanced Photon Source, , 9700 S. Cass Ave., Argonne, Illinois 60439, USA
-
- Hiroyuki Nojiri
- Institute for Materials Research 3 , Tohoku University, Sendai, Japan
-
- Yasuo Narumi
- Institute for Materials Research 3 , Tohoku University, Sendai, Japan
-
- Ulrich Welp
- Argonne National Laboratory 4 Materials Science Division, , 9700 S. Cass Ave., Argonne, Illinois 60439, USA
-
- Paul C. Canfield
- Iowa State University 5 Department of Physics and Astronomy, Ames Laboratory, , Ames, Iowa 50010, USA
書誌事項
- 公開日
- 2012-03-01
- 資源種別
- journal article
- DOI
-
- 10.1063/1.3688251
- 10.48550/arxiv.1109.6713
- 公開者
- AIP Publishing
この論文をさがす
説明
<jats:p>We present a pulsed-magnet system that enables x-ray single-crystal diffraction in addition to powder and spectroscopic studies with the magnetic field applied on or close to the scattering plane. The apparatus consists of a single large-bore solenoid, cooled by liquid nitrogen. A second independent closed-cycle cryostat is used for cooling samples near liquid helium temperatures. Pulsed magnetic fields close to ∼30 T with a zero-to-peak-field rise time of ∼2.9 ms are generated by discharging a 40 kJ capacitor bank into the magnet coil. The unique characteristic of this instrument is the preservation of maximum scattering angle (∼23.6°) on the entrance and exit sides of the magnet bore by virtue of a novel double-funnel insert. This instrument will facilitate x-ray diffraction and spectroscopic studies that are impractical, if not impossible, to perform using split-pair and narrow-opening solenoid magnets. Furthermore, it offers a practical solution for preserving optical access in future higher-field pulsed magnets.</jats:p>
収録刊行物
-
- Review of Scientific Instruments
-
Review of Scientific Instruments 83 (3), 035101-, 2012-03-01
AIP Publishing
