Reaction of a Thioaminyl Diradical with 7,7,8,8-Tetracyanoquinodimethane (TCNQ). The Formation of a Cyclophane Compound

  • Yozo Miura
    Department of Applied Chemistry, Faculty of Engineering, Osaka City University
  • Tsuguyori Ohana
    Department of Applied Chemistry, Faculty of Engineering, Osaka City University
  • Teruo Kunishi
    Department of Applied Chemistry, Faculty of Engineering, Osaka City University

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<jats:title>Abstract</jats:title> <jats:p>The reactions of thioaminyl mono- (MONOR) and diradicals (DIR) with 7,7,8,8-tetracyanoquinodimethane (TCNQ) have been investigated. The reactions of TCNQ with MONOR gave 1:2 adducts of TCNQ and MONOR in 85–88% yields, while the reaction with DIR afforded either a cyclophane compound (77%), or an alternating polymer of TCNQ and DIR (59 wt%), dependent on the structures of DIR.</jats:p>

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