Artificial Chitin Spherulites Composed of Single Crystalline Ribbons of α-Chitin via Enzymatic Polymerization

  • Junji Sakamoto
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan
  • Junji Sugiyama
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan
  • Shunsaku Kimura
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan
  • Tomoya Imai
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan
  • Takao Itoh
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan
  • Takeshi Watanabe
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan
  • Shiro Kobayashi
    Department of Material Chemistry, Graduate School of Engineering, Kyoto University, Kyoto 606-8501, Japan, Wood Research Institute, Kyoto University, Uji, Kyoto 611-0011, Japan, and Department of Applied Biological Chemistry, Faculty of Agriculture, Niigata University, Niigata 950-2181, Japan

書誌事項

公開日
2000-05-01
DOI
  • 10.1021/ma000230y
公開者
American Chemical Society (ACS)

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説明

A crystalline product of artificial chitin by chitinase-catalyzed polymerization of a chitobiose oxazoline derivative was investigated by using optical microscopy in combination with TEM and SEM techniques. Platelike single crystals of α-chitin were first formed. The crystals were gradually shaped into ribbons by the rapid growth along the a axis with the crystalline thickness being ca. 10 nm. The α-chitin ribbons then aggregated to form bundlelike or dendritic assemblies as the ribbon concentration in solution increased. They grew into spherulites by splaying and branching, which displayed birefringence with a Maltese cross by polarization microscopic observation. The present artificial chitin spherulite, in which a number of α-chitin ribbons radiated from a common center, is completely different from the helicoidal textures composed of α-chitin microfibrils which have been known so far as a typical three-dimensional organization of chitin.

収録刊行物

  • Macromolecules

    Macromolecules 33 (11), 4155-4160, 2000-05-01

    American Chemical Society (ACS)

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