Synthesis and Reactions of a Stable 1,2-Diaryl-1,2-dibromodisilene: A Precursor for Substituted Disilenes and a 1,2-Diaryldisilyne

  • Takahiro Sasamori
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Koji Hironaka
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Yusuke Sugiyama
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Nozomi Takagi
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Shigeru Nagase
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Yoshinobu Hosoi
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Yukio Furukawa
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan
  • Norihiro Tokitoh
    Institute for Chemical Research, Kyoto University, Gokasho, Uji, Kyoto 611-0011, Japan, Department of Theoretical Molecular Science, Institute for Molecular Science, Myodaiji, Okazaki 444-8585, Japan, and Department of Chemistry, School of Science and Engineering, Waseda University, 3-4-1 Okubo, Shinjuku-ku, Tokyo 169-8555, Japan

書誌事項

公開日
2008-09-26
DOI
  • 10.1021/ja8061002
公開者
American Chemical Society (ACS)

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説明

Synthesis and isolation of the stable diaryldibromodisilene, Bbt(Br)SiSi(Br)Bbt, has been accomplished for the first time. The dibromodisilene underwent substitution reactions with organometallic reagents on the low-coordinated silicon atom to afford the corresponding substituted disilenes. Furthermore, the reaction of 1 with t-BuLi afforded the corresponding 1,2-diaryldisilyne, BbtSi[triple bond]SiBbt, the characters of which were revealed by spectroscopic and crystallographic analyses.

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