How g-C<sub>3</sub>N<sub>4</sub> Works and Is Different from TiO<sub>2</sub> as an Environmental Photocatalyst: Mechanistic View

  • Jonghun Lim
    Division of Environmental Science and Engineering and Department of Chemical Engineering, Pohang University of Science and Technology (POSTECH), Pohang 37673, Korea
  • Hyejin Kim
    Division of Environmental Science and Engineering and Department of Chemical Engineering, Pohang University of Science and Technology (POSTECH), Pohang 37673, Korea
  • Jihee Park
    Division of Environmental Science and Engineering and Department of Chemical Engineering, Pohang University of Science and Technology (POSTECH), Pohang 37673, Korea
  • Gun-Hee Moon
    Division of Environmental Science and Engineering and Department of Chemical Engineering, Pohang University of Science and Technology (POSTECH), Pohang 37673, Korea
  • Junie Jhon M. Vequizo
    Graduate School of Engineering, Toyota Technological Institute, 2-12-1 Hisakata, Tempaku, Nagoya 468-8511, Japan
  • Akira Yamakata
    Graduate School of Engineering, Toyota Technological Institute, 2-12-1 Hisakata, Tempaku, Nagoya 468-8511, Japan
  • Jinwoo Lee
    Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST), Daejeon 34141, Korea
  • Wonyong Choi
    Division of Environmental Science and Engineering and Department of Chemical Engineering, Pohang University of Science and Technology (POSTECH), Pohang 37673, Korea

書誌事項

公開日
2019-12-03
資源種別
journal article
権利情報
  • https://doi.org/10.15223/policy-029
  • https://doi.org/10.15223/policy-037
  • https://doi.org/10.15223/policy-045
DOI
  • 10.1021/acs.est.9b05044
公開者
American Chemical Society (ACS)

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説明

Graphitic carbon nitride (CN) as a popular visible light photocatalyst needs to be better understood for environmental applications. The behaviors of CN as an environmental photocatalyst were systematically studied in comparison with a well-known TiO2 photocatalyst. The two photocatalysts exhibit different photocatalytic oxidation (PCO) behaviors and dependences on the experimental conditions (e.g., pH, Pt loading, and the kind of organic substrate and scavenger). The PCO of organic substrates was significantly enhanced by loading Pt on TiO2 under UV light (λ > 320 nm), whereas Pt-CN exhibited a lower PCO activity than bare CN under visible light (λ > 420 nm). While the presence of Pt enhances the charge separation in both TiO2/UV and CN/visible light systems (confirmed by transient IR absorption spectroscopic analysis), the opposite effects of Pt are ascribed to the different mechanisms of •OH generation in the two photocatalytic systems. The negative effect of Pt on CN is ascribed to the fact that Pt catalytically decomposes in situ-generated H2O2 (a main precursor of OH radical), which hinders •OH production. The production of OH radicals on CN is favored only at acidic pH but 1O2 generation is dominant in alkaline pH. The pH-dependent behaviors of reactive oxygen species generation on CN were confirmed by electron paramagnetic resonance spin trap measurements.

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