Radical Fluoroalkylation of Isocyanides with Fluorinated Sulfones by Visible‐Light Photoredox Catalysis

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  • Jian Rong
    Key Laboratory of Organofluorine Chemistry Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences 345 Ling-Ling Road Shanghai 200032 China
  • Ling Deng
    Key Laboratory of Organofluorine Chemistry Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences 345 Ling-Ling Road Shanghai 200032 China
  • Ping Tan
    Key Laboratory of Organofluorine Chemistry Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences 345 Ling-Ling Road Shanghai 200032 China
  • Chuanfa Ni
    Key Laboratory of Organofluorine Chemistry Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences 345 Ling-Ling Road Shanghai 200032 China
  • Yucheng Gu
    Syngenta, Jealott's Hill International Research Centre Bracknell Berkshire RG42 6EY UK
  • Jinbo Hu
    Key Laboratory of Organofluorine Chemistry Shanghai Institute of Organic Chemistry, Chinese Academy of Sciences 345 Ling-Ling Road Shanghai 200032 China

抄録

<jats:title>Abstract</jats:title><jats:p>The radical fluoroalkylation of isocyanides with fluorinated sulfones is enabled by visible‐light photoredox catalysis. A wide range of readily available mono‐, di‐, and trifluoromethyl heteroaryl sulfones can thus be used as efficient radical fluoroalkylation reagents under mild conditions. This method not only describes a new synthetic application of fluorinated sulfones, but also provides a new route to fluoroalkyl radicals.</jats:p>

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