Total Synthesis of (−)‐FR182877 through Tandem IMDA–IMHDA Reactions and Stereoselective Transition‐Metal‐Mediated Transformations

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書誌事項

公開日
2009-03-17
権利情報
  • http://onlinelibrary.wiley.com/termsAndConditions#vor
DOI
  • 10.1002/anie.200900097
  • 10.1002/ange.200900097
  • 10.1002/chin.200929206
公開者
Wiley

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説明

<jats:title>Abstract</jats:title><jats:p><jats:bold>Intelligent design</jats:bold>: The total synthesis of the cytotoxic (−)‐FR182877 relies on 1) tandem Diels–Alder reactions to close rings A–D (see scheme), 2) a palladium‐mediated 7‐<jats:italic>exo</jats:italic>‐trig reaction, and 3) an iridium‐mediated isomerization followed by epimerization and stereoselective reduction.<jats:boxed-text content-type="graphic" position="anchor"><jats:graphic xmlns:xlink="http://www.w3.org/1999/xlink" mimetype="image/gif" position="anchor" specific-use="enlarged-web-image" xlink:href="graphic/mcontent.gif"><jats:alt-text>magnified image</jats:alt-text></jats:graphic></jats:boxed-text></jats:p>

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