The Preparation of Potassium Octacyanomolybdate(IV) Dihydrate

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<jats:title>Abstract</jats:title><jats:p>K<jats:sub>4</jats:sub>Mo(CS)<jats:sub>8</jats:sub> · 2 H<jats:sub>2</jats:sub>O was prepared by the reduction of MOO<jats:sup>2−</jats:sup> by KBH<jats:sub>4</jats:sub> in potassium cyanide medium. The reduction proceeds during the slow addition of concentrated acetic acid. The synthesis is efficient because reduction and complexation are accomplished at the same time.</jats:p>

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