Deoxygenative Borylation of Secondary and Tertiary Alcohols

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  • Florian W. Friese
    Westfälische Wilhelms-Universität Organisch-Chemisches Institut Corrensstrasse 40 48149 Münster Germany
  • Armido Studer
    Westfälische Wilhelms-Universität Organisch-Chemisches Institut Corrensstrasse 40 48149 Münster Germany

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<jats:title>Abstract</jats:title><jats:p>Two different approaches for the deoxygenative radical borylation of secondary and tertiary alcohols are presented. These transformations either proceed through a metal‐free silyl‐radical‐mediated pathway or utilize visible‐light photoredox catalysis. Readily available xanthates or methyl oxalates are used as radical precursors. The reactions show broad substrate scope and high functional‐group tolerance, and are conducted under mild and practical conditions.</jats:p>

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