Determination of Unsaponifiable Constituents of Deodorizer Distillates by GC–MS

DOI Web Site Web Site 被引用文献1件
  • Saba Naz
    National Center of Excellence in Analytical Chemistry University of Sindh Jamshoro Pakistan
  • S. T. H. Sherazi
    National Center of Excellence in Analytical Chemistry University of Sindh Jamshoro Pakistan
  • Farah N. Talpur
    National Center of Excellence in Analytical Chemistry University of Sindh Jamshoro Pakistan
  • M. Younis Talpur
    National Center of Excellence in Analytical Chemistry University of Sindh Jamshoro Pakistan
  • Huseyin Kara
    Fen‐Edebiyat Fakültesi, Kimya Bölümü Selcuk University Kampus Konya 42075 Turkey

書誌事項

公開日
2012-01-14
権利情報
  • http://onlinelibrary.wiley.com/termsAndConditions#vor
DOI
  • 10.1007/s11746-011-2000-z
公開者
Wiley

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説明

<jats:title>Abstract</jats:title><jats:p>Deodorizer distillate is an important by‐product obtained during deodorization in the edible oil industries. It is a complex mixture of many health beneficial constituents like phytosterols, tocopherols and squalene. In the present study a simple gas chromatographic method with mass spectrometry was used for the separation, detection and quantification of different components present in the deodorizer distillate in a very short analysis time of 18 min. A simple saponification procedure without derivatization was used for their analysis followed by GC–MS analysis. Phytosterols concentration (21.27–25.53%) was the most abundant in canola and palm distillate samples whereas, squalene and tocopherol were present in concentration ranges of 2.89–13.21% and 1.29–5.81%, respectively. The present study revealed that the unsaponifiable fraction of deodorizer distillate could be used in cosmetic preparations due to its appreciable amount of bioactive constituents.</jats:p>

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