Selective Synthesis of Single‐Handed Helical Polymers from Achiral Monomer and a Mechanism Study on Helix‐Sense‐Selective Polymerization

  • Li Zhou
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China
  • Xun‐Hui Xu
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China
  • Zhi‐Qiang Jiang
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China
  • Lei Xu
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China
  • Ben‐Fa Chu
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China
  • Na Liu
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China
  • Zong‐Quan Wu
    Department of polymer science and engineering School of chemistry and chemical engineering Anhui Key Lab of Catalytic Materials and Reaction Engineering Hefei university of Technology 193 Tunxi Road, Hefei 230009 Anhui China

書誌事項

公開日
2020-11-12
権利情報
  • http://onlinelibrary.wiley.com/termsAndConditions#vor
DOI
  • 10.1002/anie.202011661
公開者
Wiley

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説明

<jats:title>Abstract</jats:title><jats:p>Inspired by the exquisite helices in Nature, fabrication of helical materials with controlled handedness has attracted considerable attention. Herein, we report on precis synthesis of single left‐ and right‐handed helical polyisocyanides through living polymerization of achiral monomers using chiral palladium catalysts under helix‐sense‐selective manner. Mechanism study revealed that the yielded helices with opposite handedness showed different activity of the living chain end. The helix with unfavored handedness was self‐terminated, while the one with favored handedness showed high activity and could undergo chain propagation to form a high molecular weight polymer with maintained single‐handed helicity.</jats:p>

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