Rhodium(III)‐Catalyzed Amidation of Unactivated C(sp<sup>3</sup>)H Bonds

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公開日
2015-09-07
権利情報
  • http://onlinelibrary.wiley.com/termsAndConditions#vor
DOI
  • 10.1002/anie.201506323
公開者
Wiley

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説明

<jats:title>Abstract</jats:title><jats:p>Nitrogenation by direct functionalization of CH bonds represents an important strategy for constructing CN bonds. Rhodium(III)‐catalyzed direct amidation of unactivated C(sp<jats:sup>3</jats:sup>)H bonds is rare, especially under mild reaction conditions. Herein, a broad scope of C(sp<jats:sup>3</jats:sup>)H bonds are amidated under rhodium catalysis in high efficiency using 3‐substituted 1,4,2‐dioxazol‐5‐ones as the amide source. The protocol broadens the scope of rhodium(III)‐catalyzed C(sp<jats:sup>3</jats:sup>)H activation chemistry, and is applicable to the late‐stage functionalization of natural products.</jats:p>

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