誘導結合プラズマ発光分析法による青銅器主成分の定量 試料溶解と溶液の安定性
書誌事項
- タイトル別名
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- ICP-AES; Sample dissolution and stability of the solution.
- ユウドウ ケツゴウ プラズマ ハッコウ ブンセキホウ ニ ヨル セイドウキ シ
- Sample dissolution and stability of the solution
- 試料溶解と溶液の安定性
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抄録
In 0.3 M HCl, tin was stable only for 1 month, but it was stable over 4 months in 1 M HCl. Thus the acidity of sample solution was kept in 1 M HCl. The sample block was drilled with tungsten carbide tip and chips of 50 mg were dissolved in 0.2 ml of H2O and 0.3 ml of HNO3 with gentle heating on a hot plate, if necessary. The white residue of metastannic acid was easily dissolved by the addition of 8.5 ml of HCl. The final solution was made up to 100 g with H2O, which was used for sequential ICP-AES determinations of Cu, Sn, Pb, Zn and Ni. These major elements in the solution were stable for at least 2 months even if the residual HNO3 was 0.5 M. The present method was successfully applied for BCS No. 183/3, Leaded Gunmetal, an ancient bronze and some recent bronzes imitated from the ancient.
収録刊行物
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- 分析化学
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分析化学 38 (4), T49-T53, 1989
公益社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390001204052300800
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- NII論文ID
- 110002904962
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- NII書誌ID
- AN00222633
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- COI
- 1:CAS:528:DyaL1MXls1KnsLk%3D
- 1:CAS:528:DyaL1MXktFKrsLY%3D
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- ISSN
- 13482246
- 05251931
- 09106340
- http://id.crossref.org/issn/05251931
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- NDL書誌ID
- 3226790
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- Web Site
- http://id.ndl.go.jp/bib/3226790
- https://ndlsearch.ndl.go.jp/books/R000000004-I3226790
- https://link.springer.com/content/pdf/10.2116/analsci.5.49.pdf
- https://link.springer.com/article/10.2116/analsci.5.49/fulltext.html
- http://www.jstage.jst.go.jp/article/analsci1985/5/1/5_1_49/_pdf
- http://www.jstage.jst.go.jp/article/bunsekikagaku1952/38/4/38_4_T49/_pdf
- http://dl.ndl.go.jp/info:ndljp/pid/10892089
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
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