Microanalysis of carbon, hydrogen, and nitrogen in air-sensitive organometallic compounds.

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  • SHIBUE Toshimichi
    Materials Characterization Central Laboratory, School of Science and Engineering, Waseda University
  • YOSHIDA Fumihiko
    Materials Characterization Central Laboratory, School of Science and Engineering, Waseda University
  • KANBE Hisashi
    Materials Characterization Central Laboratory, School of Science and Engineering, Waseda University
  • NITTA Makoto
    Department of Chemistry, School of Science and Engineering, Waseda University

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Other Title
  • 空気に敏感な有機金属化合物中の炭素，水素及び窒素の定量
  • クウキ ニ ビンカン ナ ユウキ キンゾク カゴウブツチュウ ノ タンソ スイ

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Description

A convenient, rapid and highly reproducible method has been established for the microanalysis of carbon, hydrogen and nitrogen in air-sensitive organometallic compounds. By using a combination of a gloved box technique and an aluminium pan for the sampling, samples make no contact with air or water. Furthermore, samples of the desired weight are easily available before searing up the aluminum pan. The analytical data obtained for carbon, hydrogen, and nitrogen in these air-sensitive compounds are in good agreement with the corresponding theoretical values.

Journal

  • BUNSEKI KAGAKU

    BUNSEKI KAGAKU 44 (1), 83-86, 1995

    The Japan Society for Analytical Chemistry

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