Study on proximate analysis of coal using thermobalance.
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- WATANUKI Osamu
- Hokuriku Electric Power Co. Inc.
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- MATSUBARA Akio
- 北陸電力(株)技術研究所
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- BETSUMORI Keiichi
- 北陸電力(株)富山新港火力発電所
Bibliographic Information
- Other Title
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- 熱はかりを用いた石炭の工業分析法の検討
- ネツ ハカリ オ モチイタ セキタン ノ コウギョウ ブンセキホウ ノ ケント
- 熱はかりを用いた石炭の工業分析法の検討(<特集>石炭利用と分析化学)
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Description
The accuracy of a thermogravimetric analysis (TGA) for the determination of moisture, volatiles, fixed-carbon and ash in coal was investigated. The method consists of the following 4 sequential steps: (1) preparation: Load a 50 mg sample of constant humidity base coal to a thermobalance and purge high-purity nitrogen into a furnace. (2) moisture determination: Heat the sample up to 107 °C in a nitrogen atmospher and hold it at the temperature for 10 min. (3) volatiles determination: Increase furnace temperature up to 900 °C and hold at the temperature for 7 min. (4) fixed-carbon determination: Decrease furnace temperature to 815 °C and switch furnace environment from nitrogen to high-purity oxygen. After each procedure, the weight losses of each component were measured as percentages to the total sample weight. In regard to moisture, fixed-carbon and ash contents, the results by the TGA method were in good agreement with those of JIS method. For the volatiles, however, TGA showed a little lower values than those by JIS method.
Journal
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- BUNSEKI KAGAKU
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BUNSEKI KAGAKU 34 (5), T51-T55, 1985
The Japan Society for Analytical Chemistry
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Details 詳細情報について
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- CRID
- 1390001204053252608
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- NII Article ID
- 110002909175
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- NII Book ID
- AN00222633
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- NDL BIB ID
- 3032681
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- ISSN
- 05251931
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- Text Lang
- ja
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- Data Source
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- JaLC
- NDL
- Crossref
- NDL-Digital
- CiNii Articles
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- Abstract License Flag
- Disallowed