Electron Channeling X-ray Spectroscopy and its Application to Structure Analysis of Crystalline Materials
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- MATSUMURA Syo
- 九州大学大学院工学研究院
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- SHIMADA Mikio
- 九州大学大学院工学研究院
Bibliographic Information
- Other Title
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- 電子線で今何ができるか 1.電子線結晶構造解析の最先端 チャンネリングを用いたサイト選択解析:ALCHEMI
- チャンネリング オ モチイタ サイト センタク カイセキ ALCHEMI
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Abstract
This paper first summarizes principles of electron channeling X-ray microanalysis (ALCHEMI) and then describes a recent achievement in quantitative structure analysis of MgO⋅nA12O3 spinel compounds. The orientation dependent intensity variation of emitted X-rays under dynamical electron diffraction conditions is so sensitive to lattice-ion configuration in the illuminated areas that the occupation probabilities on specific positions in the crystal lattice can be determined accurately through comparison with the theoretical rocking curves. The measurements have characterized partially disordered cation configuration in MgO⋅nA12O3 crystals as a function of composition as well as irradiation-induced disordering.
Journal
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- Nihon Kessho Gakkaishi
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Nihon Kessho Gakkaishi 47 (1), 55-60, 2005
The Crystallographic Society of Japan
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Details 詳細情報について
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- CRID
- 1390001204086979072
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- NII Article ID
- 10014463486
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- NII Book ID
- AN00188364
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- ISSN
- 18845576
- 03694585
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- NDL BIB ID
- 7266231
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- Text Lang
- ja
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- Data Source
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- JaLC
- NDL
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed