Anomalous Small-Angle X-ray Scattering Studies of Phase Separation in Bulk Amorphous Zr<SUB><B>52.5</B></SUB>Ti<SUB><B>5</B></SUB>Cu<SUB><B>17.9</B></SUB>Ni<SUB><B>14.6</B></SUB>Al<SUB><B>10</B></SUB>

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  • Anomalous Small-Angle X-ray Scattering Studies of Phase Separation in Bulk Amorphous Zr52.5Ti5Cu17.9Ni14.6Al10

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Abstract

We have performed differential anomalous small-angle X-ray scattering (ASAXS) experiments on samples of bulk amorphous Zr52.5Ti5Cu17.9Ni14.6Al10 annealed in the supercooled liquid region. We observe the development of strong small-angle scattering, associated with phase separation on the nanometer scale in the supercooled liquid. Analysis of the Zr-edge ASAXS data reveals that this phase separation is largely due to a redistribution of Zr. Continued annealing results in the nucleation and growth of Zr-rich crystalline intermetallic phases.

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  • MATERIALS TRANSACTIONS

    MATERIALS TRANSACTIONS 42 (4), 562-564, 2001

    The Japan Institute of Metals and Materials

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