Characterization of Spinel-Structured Iron Oxide Particles Synthesized by Heating α-Fe₂O₃ Platelets in Tetra-Ethylene Glycol
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- Kishimoto Mikio
- Institute of Applied Physics, University of Tsukuba
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- Asai Kei
- Department of Materials Science, Graduate School of Pure and Applied Sciences, University of Tsukuba
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- Horiuchi Akari
- Institute of Applied Physics, University of Tsukuba
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- Yanagihara Hideto
- Institute of Applied Physics, University of Tsukuba
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- Nagasaki Yukio
- Department of Materials Science, Graduate School of Pure and Applied Sciences, University of Tsukuba
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- Kita Eiji
- Institute of Applied Physics, University of Tsukuba
書誌事項
- タイトル別名
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- Characterization of Spinel-Structured Iron Oxide Particles Synthesized by Heating α-Fe<sub>2</sub>O<sub>3</sub> Platelets in Tetra-Ethylene Glycol
- Characterization of Spinel-Structured Iron Oxide Particles Synthesized by Heating α-Fe<sub>2</sub>O<sub>3</sub> Platelets in Tetra-Ethylene Glycol
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Platelet particles of α-Fe2O3 30–50 nm in size were heated in tetra-ethylene glycol to obtain spinel-structured iron oxide particles, which were confirmed by X-ray diffraction. With heating, 100 nm platelets were formed, and the proportion of the 100 nm platelets increased in comparison to 30–50 nm platelets with increasing duration of heating. In all the samples, irrespective of the heating time used during synthesis, the coercive force, which was considered to be dependent on the shape anisotropy of the platelet particles, remained nearly constant at 12.7–13.5 kA/m (160–170 Oe). The saturation magnetization initially increased and then decreased with the heating time and the maximum value observed was 80.5 Am2/kg (80.5 emu/g). The reduction and oxidation were considered to occur simultaneously during the synthesis.
収録刊行物
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- MATERIALS TRANSACTIONS
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MATERIALS TRANSACTIONS 54 (2), 222-224, 2013
公益社団法人 日本金属学会
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詳細情報 詳細情報について
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- CRID
- 1390001204248923136
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- NII論文ID
- 10031144484
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- NII書誌ID
- AA1151294X
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- COI
- 1:CAS:528:DC%2BC3sXltVKqtL0%3D
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- ISSN
- 13475320
- 13459678
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- NDL書誌ID
- 024227575
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
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- KAKEN
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- 抄録ライセンスフラグ
- 使用不可