Influence of Bath Composition on Tensile Ductility in Electrodeposited Bulk Nanocrystalline Nickel
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- Matsui Isao
- Department of Materials Science, Osaka Prefecture University
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- Takigawa Yorinobu
- Department of Materials Science, Osaka Prefecture University
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- Uesugi Tokuteru
- Department of Materials Science, Osaka Prefecture University
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- Higashi Kenji
- Department of Materials Science, Osaka Prefecture University
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We investigated the influence of bath composition on characteristics in an electrodeposited bulk nanocrystalline Ni (nc-Ni). This study was aim to establish the fabrication process of bulk nc-Ni with good tensile property. The bulk nc-Ni was electrpdeposited from a sulfate bath and a sulfamate bath. The nc-Ni was evaluated for microstructure and mechanical properties, such as microhardness, tensile strength. As a result, bulk nc-Ni obtained from a sulfamate bath exhibited enhanced tensile property (ultimate tensile strength of 1006 MPa and ductility of 8.8%) compared to that obtained from a sulfate bath. Dimple pattern was observed in fracture surface of bulk nc-Ni obtained from a sulfamate bath. However, dimple pattern and brittle fracture surface were observed in bulk nc-Ni obtained from a sulfate bath. We consider the ductility of electrodeposited nc-Ni was influenced by internal stress generated from electrodepostion. These experiments and analyses suggest that it is important to control internal stress on fabrication of bulk nc-Ni with high tensile strength and good ductility.
収録刊行物
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- MATERIALS TRANSACTIONS
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MATERIALS TRANSACTIONS 52 (2), 142-146, 2011
公益社団法人 日本金属学会
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詳細情報 詳細情報について
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- CRID
- 1390001204250547968
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- NII論文ID
- 10027837465
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- NII書誌ID
- AA1151294X
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- ISSN
- 13475320
- 13459678
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- NDL書誌ID
- 10958798
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
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- 使用不可