Evaluation of the Thermal Desorption-GC/MS Method for the Determination of Decabromodiphenyl Ether (DeBDE) in Order of a Few Hundred ppm Contained in a Certified Standard Polystyrene Sample
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- YUZAWA Tetsuro
- Frontier Laboratories Ltd.
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- HOSAKA Akihiko
- Frontier Laboratories Ltd.
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- WATANABE Chuichi
- Frontier Laboratories Ltd.
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- TSUGE Shin
- Frontier Laboratories Ltd. Nagoya University
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Abstract
Thermal desorption (TD)-GC/MS, recently developed for the determination of DeBDE in a polystyrene (PS) sample to an order of a few %, was evaluated in detail by using a certified standard PS sample containing 317 ppm of DeBDE. Not only the accuracy and precision of the results, but also the linearity of the working calibration curve were discussed in terms of the catalytic decomposition of DeBDE induced by the degrading macro-radical of the matrix polymer.
Journal
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- Analytical Sciences
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Analytical Sciences 24 (8), 953-955, 2008
The Japan Society for Analytical Chemistry
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Keywords
Details 詳細情報について
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- CRID
- 1390001204256521984
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- NII Article ID
- 130004441700
- 10025205350
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- NII Book ID
- AA10500785
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- ISSN
- 13482246
- 09106340
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- NDL BIB ID
- 9600596
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- Text Lang
- en
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- Data Source
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- JaLC
- NDL
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed