Determination of Silicon in Urine and Blood by Graphite-Furnace Atomic Absorption Spectrometry with a Nickel Chloride Modifier.
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- Kobayashi R.
- Occupational Health Service Centre
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- Okamura S.
- Occupational Health Service Centre
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- Yamada K.
- Occupational Health Service Centre
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- Kudo M.
- Occupational Health Service Centre
書誌事項
- タイトル別名
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- Determination of Silicon in Urine and B
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抄録
A method has been developed for the determination of silicon in urine and blood by graphite-furnace atomic absorption spectrometry. Nickel chloride was employed for the matrix modifier. The tolerable ashing temperature was raised to 2200°C in the presence of a matrix modifier. The urine was diluted 1+349 with distilled water and the blood was diluted 1+19 with Triton X(1%), and introduced into a pyrocoated graphite tube together with a nickel solution. Recoveries of the silicon added to the urine and the blood samples ranged from 85.5 to 89.3% for urine and 69.3 to 72.0 % for blood; the relative standard deviation was within 10% at the 10mg/l level. The silicon contents in urine and blood, determined by the proposed method, ranged from 2.6-23.7mg/l and 1.0-4.6mg/l, respectively.
収録刊行物
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- Analytical Sciences
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Analytical Sciences 13 (Supplement), 17-20, 1997
社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390001204257505536
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- NII論文ID
- 40005334940
- 130003528377
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- NII書誌ID
- AA10500785
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- ISSN
- 13482246
- 09106340
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- NDL書誌ID
- 4371120
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
- Crossref
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可