Synthesis and catalysis activity of aluminum phosphate.

  • TAKIZAWA Takashi
    Department of Applied Chemistry, School of Engineering, Tokai University
  • ISHIMOTO Yoichi
    Department of Applied Chemistry, School of Engineering, Tokai University
  • NAGAO Tomomi
    Department of Applied Chemistry, School of Engineering, Tokai University
  • MATSUSHITA Jun-ichi
    Department of Applied Chemistry, School of Engineering, Tokai University

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Other Title
  • リン酸アルミニウムの合成および触媒特性の評価

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Abstract

Catalyst activity of aluminum phosphate can be changed dramatically depending on their preparation. In this paper, the sol-gel process and precipitation process were desceibed. The characteristics of sol-gel process, fine, uniform-sized particles were obtained, and high specific surface area and high catalysis activity can be expected. As raw materials, aluminum isopropoxide and triethyl phosphate were used. Diethanolamine and 2-methoxyethanol were used as solvents. Aluminum phosphate were synthesized in three ways. Each synthesized aluminum phosphate had been dried for 24h at 353K. Dried samples had been sintered for 2h at 873K and additionally sintered for 2h at 1173K, 1273K, 1373K and 1473K in the air. The catalyst activity of sintered samples was validated by the decomposition of C2F6 and XDR analysis.

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Details 詳細情報について

  • CRID
    1390001204343052416
  • NII Article ID
    10014141307
  • NII Book ID
    AA11948435
  • DOI
    10.2978/jsas.12.81
  • ISSN
    18813917
    09155651
  • Text Lang
    ja
  • Data Source
    • JaLC
    • Crossref
    • CiNii Articles
  • Abstract License Flag
    Disallowed

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