各種クリーンアップ法とＨＲＧＣ／ＨＲＭＳを用いたポリ塩化ビフェニル（ＰＣＢｓ）の全異性体詳細分析方法

DOI Web Site 被引用文献21件

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タイトル別名
  • All Congener Specific Analytical Method for Polychlorinated Biphenyls(PCBs) with Various Chromotographic Clean-up and HRGC/HRMS.

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説明

The chromatographic clean-up and HRGC/HRMS stages of an all congener specific analytical method for PCBs were investigated in detail. Various clean-up strategies, including DMSO treatment for oily samples, alumina column clean-up for all samples, and HPLC on PGC (Porous Graphitized Column) for coplanar PCBs, were discussed. HRGC/HRMS was used in conjunction with the clean-up strategies outlined to determine the GC elution profile of all congeners. The relative merits and problems of HRGC/HRMS, HRGC (ECD), and HRGC/LRMS as the final analytical technique for the determination of PCBs were outlined. It is expected that the data presented will be useful to analytical chemists performing analyses for either total or complanar PCBs. Possible further developments in the analysis of PCBs are discussed.

収録刊行物

  • 環境化学

    環境化学 5 (3), 647-675, 1995

    一般社団法人 日本環境化学会

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詳細情報 詳細情報について

  • CRID
    1390001204369579648
  • NII論文ID
    130004162967
  • DOI
    10.5985/jec.5.647
  • COI
    1:CAS:528:DyaK2MXptFWrsrw%3D
  • ISSN
    18825818
    09172408
    http://id.crossref.org/issn/14482517
    http://id.crossref.org/issn/09172408
  • Web Site
    http://www.jstage.jst.go.jp/article/jec1991/5/3/5_3_647/_pdf
  • 本文言語コード
    ja
  • データソース種別
    • JaLC
    • Crossref
    • CiNii Articles
  • 抄録ライセンスフラグ
    使用不可

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