書誌事項
- タイトル別名
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- Rapid Analysis of PCB in Electrical Insulating Oil by Heating of Multi-Layer Silica Gel Column/Alumina Column
- カネツ タソウ シリカゲル カラム アルミナカラム オ モチイタ デンキ ゼツエンユチュウ ノ PCB ジンソク ブンセキホウ
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The rapid analysis of PCB by heating of multi-layer silica gel column / alumina column was applied to electrical insulating oils (JIS C2320-1999 Class JIS 1-7 oils) and DOP (Dioctyl phthalate) which might be used for some capacitors. The results indicated that most of oil components were removed by the same analysis technique using multi-layer silica gel column with heating at 85 °C for 60 min without depending oil class. Oil components in JIS 4, 5, 6 oils and DOP were removed by only sulfuric acid coating silica gel treatment with heating, and also those in JIS 1, 2, 3 and 7 oils were removed by addition separation treatment of alumina to sulfuric acid coating silica gel treatment. Furthermore, quantitative capability and repeatability (n =3) of PCB concentration in JIS 1-7 oils and DOP were evaluated by GC/ECD, GC/QMS and GC/MS/MS, indicating those deviations were less than ±20 % from a truth value, and also those variations were less than15 % for all of oils and measurement instruments.
収録刊行物
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- 環境化学
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環境化学 20 (4), 357-370, 2010
一般社団法人 日本環境化学会
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詳細情報 詳細情報について
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- CRID
- 1390001204370147072
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- NII論文ID
- 10027660615
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- NII書誌ID
- AN10547099
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- COI
- 1:CAS:528:DC%2BC3MXovVCkug%3D%3D
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- ISSN
- 18825818
- 09172408
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- NDL書誌ID
- 10946755
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
- NDL
- Crossref
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- 抄録ライセンスフラグ
- 使用不可