書誌事項
- タイトル別名
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- Rapid Determination of Hexamethylenetetramine in River Water by Liquid Chromatograph-Tandem Mass Spectrometer
- エキタイ クロマトグラフィー/タンデムガタ シツリョウ ブンセキケイ オ モチイル カセン スイチュウ ヘキサメチレンテトラミン ノ ジンソク テイリョウ
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We developed a simple and fast determination method of hexamethylenetetramine (HMT) by using liquid chromatography/tandem mass spectrometry to evaluate its concentration in river water. Well-defined peaks of HMT were obtained by using a hydrophilic interaction column. A calibration curve showed good linearity (R2 = 0.999). The instrumental detection limit and the instrumental quantification limit were 0.06 μg L−1 and 0.16 μg L−1, respectively. Only filtration was adopted for river-water sample pretreatment; the detection limit of HMT was calculated to be 0.12 μg L−1. The recoveries of HMT added to pure water and river water ranged from 102% to 106% and from 92% to 104%. HMT was detected from 6 of 13 grab samples taken from Tone River system between May 18th and May 20th; the maximum concentration was 150 μg L−1.
収録刊行物
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- 分析化学
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分析化学 62 (1), 47-50, 2013
公益社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390001204660583168
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- NII論文ID
- 10031139090
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- NII書誌ID
- AN00222633
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- COI
- 1:CAS:528:DC%2BC3sXit1altLg%3D
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- NDL書誌ID
- 024250361
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- ISSN
- 05251931
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
- NDL
- Crossref
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- 抄録ライセンスフラグ
- 使用不可