Crystal Structure of 1-N-Methyl[2,2']spiro-acenaphthene-1'-one[3,2"]spiro-cyclohexane-1"-one-4-[p-methylphenyl]pyrrolidine
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- PALANI K.
- Department of Crystallography and Biophysics, University of Madras
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- POORNACHANDRAN M.
- Department of Organic Chemistry, University of Madras, Guindy Campus
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- RAGHUNATHAN R.
- Department of Organic Chemistry, University of Madras, Guindy Campus
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- NETHAJI M.
- Department of Inorganic and Physical Chemistry, Indian Institute of Science
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- PONNUSWAMY M. N.
- Department of Crystallography and Biophysics, University of Madras
Description
The title compound (C28H27NO2) crystallizes in monoclinic space group P21/c with a molecule in the asymmetric unit. The structure was solved by direct methods and refined by full-matrix least-squares procedures to final R = 0.0788 and wR = 0.2022 using 3083 reflections. The pyrrolidine and cyclohexane rings adopt envelope and chair conformations, respectively. The molecules are stabilized by C-H…O type intra and intermolecular interactions in addition to van der Waals forces.
Journal
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- Analytical Sciences: X-ray Structure Analysis Online
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Analytical Sciences: X-ray Structure Analysis Online 22 X85-X86, 2006
The Japan Society for Analytical Chemistry
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Keywords
Details 詳細情報について
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- CRID
- 1390001205200427904
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- NII Article ID
- 130004937310
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- ISSN
- 13482238
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- Text Lang
- en
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- Data Source
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- JaLC
- Crossref
- CiNii Articles
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- Abstract License Flag
- Disallowed